GCMS analytical results for sample AE03830, March 29, 2002

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Data File : C:\HPCHEM\l\DATA\MAR2202\3830.D Vial: 11 Acq On : 23 Mar 2002 3:57 am Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

38.86 0.68 ug/1 48242 Perylene-dl2 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,1,1,5,7,7,7-Heptam0thyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 2 3,6-Dioxa-2,4,5,7-tetrasilaoctane , 294 C10H3002Si4 004342-25-0 25 3 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 12 4 Benzophenone-2,4 5-tricarboxylic a 356 C19H1607 000000-00-0 10 Abundance Scan 3683 (38.857 min): 3830.D (-) m/ Z 73.00 100.00% 73 147 221 5000- 281 355 . 40 253 429

m/z-> 96 ,,, ,i........... I I' ” ' I" •»I • I fl j lit 11 l Or TTTTTT1 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 38.60 38.80 39.00 39.20 m/z 147.00 57.00% Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 147 5000 267 A AC , AA AA/ 355 429 38.60 38.80 39.00 39.20 45 207 m/z 221.05 51.19%

m/z-> l ■ ■ ■ ’ I' '"I I ... .. L.. p . i । j 111 • ।. ।. 111 • i 11 n r. p 1111 ।. i. > p ।.. p n 111. । • |> • >i । ■... p ... p . h p f. • p 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #41682. 3.6-Dioxa-2.4;5,7-tetrasilaoctane, 2.2.4.4.5.5.Z.7- 147 221 ■ i • • 73 38.60 38.80 39.00 39.20 5000 m/z 281.05 33.06% 191 117 279 111' " P 11111 rrrp i 11 p 1111 ‘I‘‘‘ITETTTT‘T < । p ... P . <. p .. i p i m । .th । n 111 I" " i WAWW MWWWA 'm/z--> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 7 147 38.60 38.80 39.00 .39.20 281 m/z 355.05 31.61% 5000-

369

m/z-> —LAI, 1 338 40 60 80 100 120 -40160 180 200 220 240 260 280 300 320 340 360 380 400 420 1 T T 1 ’ 1 ' I • ■ 38.60 38.80 39.00 39.20

3830.D GCMS0308.M Tue Mar 26 14:58:53 2002 Page 2

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