GCMS analytical results for sample AE03830, March 29, 2002

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Data File C:\HPCHEM\1\DATA\MAR2202\3830.D Vial 11 Acq On 23 Mar 2002 3:57 am Operator Sample gc/ms scan 2/20 Inst GC/MS 209 Mise Multiplr 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.86 0.43 ug/1 60824 Naphthalene-d8 15.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 59 2 N- (Trifluoroacetyl) -N,O,O' ,0' ‘-tetr 553 C22H42F3NO4Si4 000000-00-0 43 3 Phenethylamine , N-methyl - . beta . , 3,4 399 C18H37NO3Si3 010538-85-9 37 4 N-(Trifluoracetyl)-0,01,0"-tris(tri 495 C2QH36F3NO4Si3 000000-00-0 35 Abundance Scan 1069 (14.859 min): 3830.D (-) m/z. 73.00 100.00% 73

5000-

45 154 193 267 355 .. 4.. ____ 14.60 14.80 15.00 15.20 ' — ..... 323 ..................... I m/z 267.00 42.37% m/z-> 50 100 150 .200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 - 5000- 14.60 14.80 15.00 15.20 m/z 355.05 40.17% 207 323 ■ • i miz—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-fTriflucroacetyD-N O.O .O -tetrakisitrinieiriylsi 73. - / 18 355 14.60 14.80 15.00i 15.20- 5000 m/z. 356.05 13.05%

45 147 193 267 । 538 ■ ■ i ■ • • ■ । ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 ' 14.60 14.80 15.001 15.20 m/z 268.00 10.06% 5000- 355 44 147 193 267 294 m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

3830.D GCMS0308.M Tue Mar 26 14:58:49 2002 Page -1

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