GCMS analysis results for sample AE06450, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6450.D Vial: 8 Acq On : 17 Apr 2002 3:05 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 9,12,15-Octadecatrienoic acid, Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 42.67 0.59 ug/1 44645 Perylene-dl2 37.87 Hit# Of 5 Tentative ID MW MolForm CAS# Qual ___ ,_________ 1 9,12,15-Octadecatrienoic acid, 2,3- 496 C27H5204Si2 055521-22-7 10 2 (5H)Pyrido[1,2-c]pyrrolo[1,2-a]pyri 222 C14H26N2 000000-00-0 9 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 9 4 3 - Isopropoxy-1/, 1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 9 Abundance 1 Scan 4098 (42.669 min): 6450.D (-) m/z 73.00 100.00%

2 73 147

221 5000 355 281 96 40 429 ' 1 I r 1 1 1 ! '' 1 1 I 1 1 1 1 1 1 1 42.40 42.60 42.80 43.00 191 m/z 147.00 95.30% I 'I 1 1 1 ' 1 1 ' i 1 ■ i 1 1 1 ■ i 1 ' 1 ' i ■ ■ ■ ■ i ■ ■ ' ' i 1 — / mfe-> 50 100 150 200 250 300 350 400 450 Abundance #58836: 9,12,15-Octadecatrienoic acid, 2,3-bis[(trimethylsi 73 147

5000 109 220 AAAAMAAN Ji "1/ rrri 1 , 1 I TT 42.40 42.60 42.80 43.00 191 281 m/z 220.95 57.84% 249 303 377 -I——— ________ L______ 452 I 1 1 1 1 1 1 i ‘ m/z-> 50 100 150 200 250 300 350 400 450 Abundance #28170: (5H)Pyrido[1,2-c]pyn’olo[1,2-a]pyrimidine, decahydr 193 221

152 42.40 42.60 42.80 43.00 5000 96 m/z 354.95 43.76%

' 1 i , 123 I _ TITl 1 1 ' 1 1 111 r 1 1 T । । ' i TBBIT Tnd 1d ! • TII mlz—> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 42.40 42.60 42.80 43.00 m/z 281.00 32.27% 355 5000 267 AWA"Warun ...............................207 _ 323 , I m/z—> 50 100 150 200 250 300 350 400 450 42.40 42.60 42.80 43.00

6450.D GCMS0412.M Thu Apr 18 09:11:37 2002 Page 5

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