Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
NYC-WTC_000039469–000039496Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 1 Cyclotrisiloxane, hexamethyl - Concentration Rank. 20 R.T. EstConc Area Relative to ISTD R.T. 7.59 0.31 ug/1 39082 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 cyclotrisiloxane , hexamethyl- 222 C6H1803Si3 000541-05-9 78 2 Arsenous acid,/tris(trimethylsilyl) 342 C9H27AsO3Si3 055429-29-3 39 3 1H-Isoindole-1, 3 (2H) -dione, 2-butyl 207 C12H17NO2 054934-85-9 9 4 Hexahydropyridine, 1-methyl-4-[4,5- 207 C12H17NO2 000000-00-0 5 Abundance I Scan 278 (7.594 min): 6430.D (-) m/z 206.95 100.00% 207
5000
1 1 1 ' 1 ' 1 1 ' ‘ ‘ I ' 1 1 1 1 1 ( 96 7.20 7.40 7.60 7.80 8.00 43 59 133 163177121 mlz-> — 40 60 1 r 4 TOTTg 80 100 120 140 160 180 200 220 240 260 280 300 320 11 ।'11 * ।11 ■11 11111 ''' | 111' I'1 m/z 208.00 25.16% Abundance #70586: Cyclotrisiloxane, hexamethyl- 207 h 5000 1 I 1 ' 1 ' 1 1 ' ' 1 I ■ ‘ 1 1 1 1 ' ’ ' 1 1 1 7.20 7.40 7.60 7.80 8.00 m/z 209.00 14.67% 96 119133147 1631771] mfe-> Abundance 40 75 ■ ■ i ■ ■ ■ ■ । • ■ ■ ■ । ■ 60 80 ' 1 ' I ' '' ' 1 1' ' 1 11' ' 1 I 1 ' 1 1 11 f 1 n T111‘1111111011111"IIITETTITTT 100 120 140 160 180 200 220 240 260 280 300 320 #48300: Arsenous acid, tris(trimethylsilyl) ester 207 wA i 1 1 ■ 1 1 1 7.20 7.40 7.60 7.80 8.00 5000 m/z 95.90 12.94%
73 105 133, 191 44 TI . 1..... L L 147 223 239 ' ■ i ■ • ■ ■ i ■ ■ ■ ■ । 1 ■ ■ • । > ■ ■ ■ । । । 327 ■ mz—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #24616:1 H-Isoindole-1 ,3(2H)-dione, 2-butyl-4,5,6,7-tetrahy 11111/-/-11/1/1/1/T71/LIIOIIIIT 207 7.20 7.40 7.60 7.80 8.00 79 m/z 190.90 10.33% 5000 152 W 124 178192 1 1 । 1 >'11 11 ■ ■ i ■ ■ ■ ■ । ■11 ■ ■ TH I I I I I I I I I I II I I I I I I I I I I [ I I I I I I I I I I I I I I I IIECEE[TT*I111IE1111ITIT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 720 7.40 7.60 7.80 8.00
6430 .D GCMS0412,M Thu Apr 18 09:09:18 2002 Page 1
NYC-WTC_000039476
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NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039588
Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder