GCMS reference results for sample AE06430, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1702\REF1.D Vial: 4 Acq On : 17 Apr 2002 11:11 am Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1715:352002 iQuant Results File: GCMS0412.RES.

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 501862 20.00 ug/1 -0.03 10) Naphthalene-d8 15.85 136 1764033 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 978020 20.00 ug/1 -0.02 30) Phenanthrene-dlO 25.59 188 1372229 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 783875 20.00 ug/1 -0.04 45) Perylene-dl2 37.87 264 467419 20.00 ug/1 -0.05

System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 30.66 235 58580 3.67 ug/mL 0.17 Spiked Amount 5.000 Recovery = 73.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.88 74 70450 6.45 ug/1 98 3) bis(2-Chloroethyl)ether 11.62 93 167125 9.83 ug/1 99 4) 1,3-Dichlorobenzene 12.11 146 146191 8.34 ug/1 100 5) 1,4-Dichlorobenzene 12.26 146 152307 8.63 ug/1 98 6) 1,2-Dichlorobenzene 12.77 146 150523 9.19 ug/1 100 7) 2,21-oxybis(1-Chloropropan 13.09 45 233401 9.94 ug/1 98 8) N-Nitroso-di-n-propylamine 13.48 70 101870 9.14 ug/1 98 9) Hexachloroethane 13.63 117 42810 6.62 ug/1 98 11) Nitrobenzene 13.89 77 138828 8.98 ug/1 99 12) Isophorone 14.54 82 269399 9.21 ug/1 99 13) bis(2-Chloroethoxy)methane 15.22 93 196676 10.32 ug/1 100 14) 1,2,4-Trichlorobenzene 15.74 180 130464 9.73 ug/1 98 15) Naphthalene 15.90 128 451441 10.64 ug/1 99 16) Hexachlorobutadiene 16.44 225 47360 7.06 ug/1 99 18) Hexachlorocyclopentadiene 18.64 237 6510 1.51 ug/1 89 19) 2-Chloronaphthalene 19.41 162 274790 10.65 ug/1 97 20) Dimethylphthalate 20.49 163 342540 11.52 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 57272 8.06 ug/1 95 22) Acenaphthylene 20.68 152 392251 10.87 ug/1 100 23) Acenaphthene 21.24 153 292268 11.39 ug/1 100 24) 2,4-Dinitrotoluene 21.88 165 61696 6.59 ug/1 97 25) Diethylphthalate 22.62 149 325465 11.41 ug/1 98 26) 4-Chlorophenyl-phenylether 22.78 204 155296 12.27 ug/1 99 27) Fluorene 22.76 166 315358 11.61 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.25 77 272441 9.03 ug/L 95 31) N-Nitrosodiphenylamine 23.17 168 77602 6.80 ug/1 96 32) 4-Bromophenyl-phenylether 24.25 248 82833 12.43 ug/1 95

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0412.M Wed Apr 17 15:36:55 2002 Page 1

NYC-WTC_000039450