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GCMS reference results for sample AE06430, April 2002

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Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.

NYC-WTC_000039445–000039452

Folder label: “GCMS X 3/19/02 A 4/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR17O2\REF1.D Vial: 4 Acq On : 17 Apr 2002 11:11 am Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1715:352002 <Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.68 284 105141 13.34 ug/1 98 34) Phenanthrene 25.65 178 434632 12.26 ug/1 99 35) Anthracene 25.78 178 365561 10.49 ug/1 99 36) Di-n-butylphthalate 27.56 149 524368 11.83 ug/1 99 37) Fluoranthene 29.28 202 402139 11.28 ug/1 95 4 0) Pyrene 29.95 202 412292 13.09 ug/1 98 41) Butylbenzylphthalate 32.08 149 172190 11.18 ug/1 100 42) Benzo(a)anthracene 33.58 228 243055 11.13 ug/1 98 43) Bis(2-ethylhexyl)phthalate 33.86 149 207971 10.55 ug/1 97 44) Chrysene 33.71 228 273411 12.62 ug/1 99 46) Di-n-Octylphthalate 35.59 149 212103 7.68 ug/1 # 98 47) Benzo(b)fluoranthene 36.69 252 201270 11.28 ug/1 99 48) Benzo(k)fluoranthene 36.75 252 216823 12.48 ug/1 97 49) Benzo(a)pyrene 37.67 252 126447 8.60 ug/1 99 50) Indeno(1,2,3-cd)pyrene 41.95 276 148606 10.03 ug/1 99 51) Dibenz(a,h)anthracene 42.02 278 131657 11.66 ug/1 97 52) Benzo(g,h,i)perylene 43.18 276 145475 11.77 ug/1 97

(#) = qualifier out of range (m) = manual integration REFl.D GCMS0412.M Wed Apr 17 15:36:56 2002 Page 2

NYC-WTC_000039451

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NYC-WTC_000039451Source: NYC Law Department, mirrored locally

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