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GCMS data file for sample AE05904, March 2002

Machine-extracted title · confidence 100%

Raw data file printout from GCMS analysis of sample AE05904 showing chromatographic peaks and retention times.

NYC-WTC_000039068–000039075

Folder label: “GCMS X 3/14/02 A 3/17/02

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Scanned page image, NYC-WTC_000039074
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report e Data File : C:\MSDCHEM\1\DATA\031702\5910.D vial: 20 Acq On : 18 Mar 2002 1:56 am Operator: McLean Sample : 3/14/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 1-Propanamine (CAS) $$ n-Pr... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

13.10 1.25 ug/L 5573 Naphthalene-d8 13.03

Hit# of 5 Tentative AD MW MolForm CAS# Qual

1 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 53 2 3-Heptanol, 4-methyl- 13 0 C8H18O 014979-39-6 38 3 3-Hexanol, 4-methyl- $$ 2-Ethyl-... 116 C7H160 000615-29-2 38 4 Butanoic acid, 3-hydroxy-3-methy... 132 C6H12O3 006149-45-7 36 Abundance Scan/1105 (13.099 min): 5910.D (-) m/ z 59.10 100.00%! 59

5000

83 T ITT ■ । ■ * • ■ । ■ i 12.80 13.00 13.20 1 3.40 , 70 , 101 116 141 m/z 83.10 22.34% 0- '11" ■ ■ i ■1'11'" ■ i ■" ■ i'44 .... 111111 — Hmm r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #654:1-Propanamine (CAS) $$ n-Propylamine $$ Propylamine ... 59

41

5000 — y M y, A 12.80 13.00 13.20 13.40 m/z 58.10 21.26%

- 5 0 III ITTT i" " i i ■ ■" i1 ■ ■11" ■ ■ i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #26892: 3-Heptanol, 4-methyl- 59

, .....—MA 12.80 13.00 13.20 13.40 m/z 56.10 15.51% 5000

27 41 83 101 70

rn/z-> 0 TTIT 94151 a 15 . । ritr । .. r. 129 i। 91 10 20 30 40 50 60 70 80 90 100 110 120 130 140 | 112 , Abundance #17030: 3-Hexanol, 4-methyl- $$ 2-Ethyl-3-pentanol $$ 4-Me... TTTTfrtr 59 T T 12.80 13.00 13.20 13.40 m/z 101.10 8.03

5000 41 31 69 87

n/z-> 0 TTI’ 15 #41—5tl 98 . । Trt ! ... I । .... p...! .... । ... I । .... । 10 20 30 40 50 60 70 80 90 100 110 120 130 140 1 1 I' 1 ■ ■ i ' 1 12.80 13.00 13.20 13.40

5910.D 5080302.M Wed Mar 20 11:30:58 2002 Page 4

NYC-WTC_000039074

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NYC-WTC_000039074Source: NYC Law Department, mirrored locally

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