GCMS scan report for sample AE05910, March 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\031702\5910 .D Vial: 20 Acq On : 18 Mar 2002 1:56 am Operator: McLean Sample : 3/14/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 1-Propanamine (CAS) $$ n-Pr... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 13.10 1.25 ug/L 5573 Naphthalene-d8 13.03

Hit# Of 5 Tentative AD MW MolForm CAS# Qual

1 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 53 2 3-Heptanol, 4-methyl- 130 C8H180 014979-39-6 38 3 3-Hexanol, 4-methyl- $$ 2-Ethyl-... 116 C7H160 000615-29-2 38 4 Butanoic acid, 3-hydroxy-3-methy... 132 C6H12O3 _____ 006149-45-7 36 Abundance Scan/1105 (13.099 min): 5910.D (-) m/z 59.10 100.00% 59

5000

83 TTPn 12.80 13.00 13.20 13.40 , 70 , 101 116 141 m/z-> 1— ------- 0- ___________________________ j '' i " " i •" ' i " ■ ■ i" ' < i' ■1 10 20 30 40 50 m/z 83.10 22.34% 60 70 80 90 100 110 120 130 140 Abundance #654: 1-Propanamine (CAS) $$ n-Propylamine $$ Propylamine ... 59

41

5000 — y Muq, 4 , 12.80 13.00 13.20 13.40 m/ z 5’3.10 21.26%

m/z-> 01 TTTTTTTT 51 TT ''I" TI " ’' i'11' P i'' "i' ■ •' i "'' i' ■'' I 10 20 30 40 50 I60 70 80 90 100 110 120 130 140 Abundance #26892: 3-Heptanol, 4-methyl- 59 ___ ------------ 12.80 13.00 13.20 13.40 5000 m/z 56.10 15.51%

27 41 101 83 |, 51 | , 70 | 15 j ...... ,91 I 112 129 0- - 1 TId ’T' 111'11111 ' f'11' i11" r ■ " i " " r " ■ i m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #17030: 3-Hexanol, 4-methyl- $$ 2-Ethyl-3-pentanol $$ 4-Me... TTIOTT—TTTT1r 59 12.80 13.00 13.20 13.40 m/z 101.10 8 03%

5000 41 31 69 87

m/z-> 15 4451 O-TT"'| 11'' I l l ' — 10 98 TTTTTT TT TTOIUITTIT 20 30 40 50 60 70 80 90 100 110 120 130 140 1 1 p ' ' ■ p ' 12.80 13.00 13.20 13.40

5910.D 5080302.M Wed Mar 20 11:30:58 2002 Page 4

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