GCMS unknowns report for sample AE02561, March 2002

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Data File : C:\HPCHEM\l\DATA\MAR1902\2561.D Vial: 20 Acq On : 20 Mar 2002 11:43 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 1-Monolinoleoylglycerol trimet Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

37.39 0.58 ug/1 57129 Perylene-dl2 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 28 2 3 - Isopropoxy-1,1,4 1 / 7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 17 3 Trisiloxane, 1,1, 1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 17 4 Silanamine, N-/[2,6-dimethyl-4-[ (tri 281 C14H27NOSi2 072088-09^-6 10 Abundance - Scan 3524 (37.395 min): 2561.D (-) m/ z 73.00 “ 100.00% 73

5000 147 221

281 355 429 37.00 37.20 37.40 37.60 37.80 44 , , ‘ ■ i ' ' ' ' i ' — 1934 253, [ | 327, | m/z 221.05 46.65% m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether 73

207 5000 147

J 37.00 37.20 37.40 37.60 37.80 34 103 281 m/z 14 6.995 45.66%

m/z--> 50 100 150 200 250 L 300 350 325 400 450 42 500 550 Abundance 73 A LWAWPA MAM 4 r VM i 37.00 37.20 37.40 37.60 37.80 5000 m/z 355.0 21.52% 147 221 281 327 415 519 561 m/z-> 50.. 100 150 200 250 300 350 400 450 500 550 Abundance #52459: Trisiloxane, 1,1,1,5,5,,5-hexamethyl-3,3-bis[(trimet i ■ ■ ■ ' i ■ ■ AA । . T ! rVt- i । 'f i 73 147 37.00 37.20 37.40 37.60 37.80 281 m/z 281.00 21.18% 5000

369 NAMMW W/wi —P 1 I r 1 r —, 1 r r r 207 I 1 r 249, 1t1. 338 | m/z-> 50 100 150 200 250 300 350 ' 400 ' 450 500 550 ' 37.00 37.20 37.40 37.60 37.80

2561.D GCMS0308.M Thu Mar 21 14:17:54 2002 Page 8

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