NYC 9/11 Public Portal Document
Data File : C:\HPCHEM\1\DATA\MAY1002\10432.D Vial: 29
Acq On : 11 May 2002 5:25 pm Operator:
Sample : gc/ms scan 5/2 Inst : 2 09
Mise : Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 2 1-Monolinoleoylglycerol trimet Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
36.07 1.29 ug/1 50506 Perylene-dl2 37.83
Hit# of 5 Tent a. ve ID MW MolForm CAS# Qual
1 1-Monolinoleo glycerol trimethylsi 498 C27H54O4Si2 054284-45-6 42
2 3-Isopropoxy/1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 23
3 3-IsopropoXy-11111,5,5,5-hexamethyl 354 C12H3404Si4 072182-11-7 14
4 Butanoic acid, 3-methyl-2-[ (trimeth 262 CllH26O3Si2 055124-92-0 12
Abundance
A Scan 3386 (36.068 min): 10432.D (-) m/z 73.10 100.00%
5000 147
221
281 355 I I | ! !
35.80 36.00 36.20 36.40
1 '
44 1 191 250 , 253, I ।... 1I .... 429
T..........
i । 1 ' ' l ‘ ‘ ‘ ' i ' 1 ' 1 1 1 1 1 1 i ■ 1 1 ' i 1 1 1 1 i 1 ■ 1 1 i 1 1 ' 1 i 1 1 1 ■ i ' 1 1 • i 1 1 m/z 147.05 49.08%
m/z—> 50 100 150 200 300 350 400 450 500 550
Abundance #58871: 1-Monolinoleoylglycerol trimethylsilyl ether
73
207
5000 147 TT
W, AAii
35.80 36.00 36.20 36.40
34 103 m/z 221.10 29.12%
281 A
m/z->
1 ■
50 100
JI ... 1 .. .17 ... 395, . 482 ...550
150 200 250 300 350 400 450 500
Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
73 I Y i''11111
35.80 36.00 36.20 36.40
5000 m/z 281.00 19.98%
147
221 281 327
.I 1g 415 519 561
। 1’1—/’I/*/III*
' 1 1 i 1 ' 1 ■ i 1 1 1 1 । ■ 1 ‘ 1 । 1 ■ 1 1 । 1 ‘
m/z-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #49645:3-lsopropoxy-1,1,1,5,5,5-hexamethyl-3-(trimethylsil i ' ' ' ' l ' ' 1 ' i ' '
73 35.80 36.00 36.20 36.40
281 m/ z 3 55.10 16.66%
5000 207
339
133 ,— 249
...... ........133 1771 1 ... 1 1
1 1 1 1 1 1 1 I 1 1 1 ' I ‘ 1 1 1 i ' ' ‘ ' i ' ' ' ' i ' 1
m/z—> 50 100 150 200 250 300 350 400 450 500 550 35.80 36.00 36.20 36.40
10432 .D GCMS0510,M Thu May 16 10:20:28 2002 Page 2
NYC-WTC_000045231
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