GCMS analysis results for sample AE10432, May 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\MAY1002\10432.D Vial: 29 Acq On : 11 May 2002 5:25 pm Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

37.29 2.09 ug/1 82047 Perylene-dl2 37.83

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 40 2 3-(3-Hydroxypheny1) -3-hydroxypropio 398 C18H3404Si3 000000-00-0 28 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 25 4 1,1,/) 3,5,5,7,7,7-Nonamethyl-3-(tri 384 C12H3604Si5 038146-99-5 25 Abundance, Scan 3519 (37.287 min): 10432.D (-) m/ z 73.10 100.00% 73

5000 147 221 281 355 । ■ i ■ ■ < - । ■

191, 1327 1.4?............ 37.00 37.20 37.40 37.60 45 1" ' T I | I I I" I 1 | I T ‘ i i 1 1 m/z 147.05 46.79% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance

5000 73 #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim

147 _.. K. . t I r ] I 1 1 I

37.00 37.20 37.40 37.60 | I I I I | I I 1 1 | i I i f

m/z 221.10 33.80% 1 1 i ■ ' i । । । i । । r-1 i i-—। 221 i r i-—i ] i 221 327 i r i । i 1 1 i i i i 415 ] 11 । i [ i i । 519 561 i [ i 1 । CTuT m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #53668: 3-(3-Hydroxyphenyl)-3-hydroxypropionic acid, tri-TMS 73 267 I I I | I I I I | I ! I I | ill i TTT 37.00 37.20 37.40 37.60 5000 147 m/z 355.10 17.48%

207 398 47 293 341 1 ' I ' ' ' 1 1 ' 1 1 i 1 —PT m/z-> 50 100 150 200 300 250 350 400 450 500 550 Abundance #71005: Ethanedioic acid, bis(trimethylsily!) ester 1 1 ' 1 1 ' 1 1 1 i 1 1 ' ■ i 1 1 ' 1 I 73 37.00 37.20 37.40 37.60 m/ z 281.00 16.73% 147 5000

45 |I1 ' 1 i ' ' IIIIIIn 117. , 190 219 /’a))/ ' 1 1 1 ‘ m/z—> 50 100 150 200 250 300 350 400 450 500 550 37.00 37.20 37.40 37.60

10432.D GCMS0510.M Thu May 16 10:20:29 2002 Page 3

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