GCMS analysis results for sample AE10432, May 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\MAY1002\10432.D Vial: 29 Acq On : 11 May 2002 5:25 pm Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

38.73 2.82 ug/1 110561 Perylene-dl2 37.83 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7, -Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 32 2 1-Monoli leoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 25 3 Silanami ne, N- [2,6-dimethyl-4-[(tri 281 C14H27NOSi2 072088-09-6 18 4 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 Abundance/ Scan 3676 (38.726 min): 10432.D (-) m/z 73.10 100.00%

147 5000 221

281| 355 43 ■ i 96 193 253 ! ll i 1 327 I.,, 429 — 38.40 38.60 38.80 39.00 m/z 147.05 50.89% m/z-> 50 100 150 200 250 :300 350 400 450 Abundance #56714:1,1t1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73

147 5000 267 ""1141’474’’11111111II 355 38.40 38.60 38.80 39.00 429 45 207 m/z 221.10 42.06%

m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1 -Monolinoleoylglycerol trimethylsilyl ether 73

T-' ' 1 ■ । 1 1 1 1 I ' 1 1 1 I 38.40 38.60 38.80 39.00 207 5000 147 m/ z 355.10 21.62% 34 103 281 | 395 / I 482 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #39584: Silanamine, N-[2,6<iimethyl-4-[(trimethylsilyl)oxy] A 1’111 ’ 1’’’I ' 1 1 ' I ' 1 ' 1 1 73 38.40 38.60 38.80 39.00

7 281 209 5000 45 251 179 125 147 D I ' 111 ' 1 i I - 1 '' I 1 m/z—> 50 100 150 200 250 300 350 400 450 38.40 38.60 38.80 39.00

10432.D GCMS0510.M Thu May 16 10:20:29 2002 Page 4

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