GCMS analysis results for sample AE10432, May 2002

NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\1\DATA\MAY1002\10432.D Vial: 29 Acq On : 11 May 2002 5:25 pm Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Trisiloxane, 1,1,1,5,5,5-hexam Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

40.47 2.64 ug/1 103262 Perylene-dl2 37.83

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Trisiloxane,1, 1,1,5,5,5-hexamethyl 3 84 C12H3 604Si5 003555-47-3 38 2 Ethanedioicacid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 12 3 3-Isopropoxy-1, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 12 4 l,l,l,5<V,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12 Abundance Scan 3866 (40.467 min): 10432.D (-) m/z 73.10 100.00% 73

147 5000 221 281 355 1 I ' 1 429 40.20 40.40 40.60 40.80

m/z-> 43 li 11 ■ 1 । 1 1 ' । । ■ > 50 100 +191 150 200 hi ।253 250 || l , .r ----------- ii r t । । i i r । ।

300 350 1l 1

400 450 500 550 m/z 147.05 58.81% Abundance ,#74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 A A MV . 5000 I I 1 1 1 1 1 1 [ ‘ I ' "I ... I 40.20 40.40 40.60 40.80 281 m/z 221.10 44.70%

m/z-> 50 4 45 ■ 117 ■iii'ii1

100 . 150 207 ' ■ i ■ ' 200 250 ' 249 1 1 ''' 369 .............. |......................................... 1 । । ■ । 1 I 1 7 । । । ' i 1 । I । । । ■ । ' ■ । ' i 1 1 300 350 400 450 500 550

07 Abundance #71006: Ethanedioic acid, bis(trimethylsilyl) ester 73 । । । । | 1 '' 3" ! ■ I I I | ! I ! TI 1111 147 40.20 40.40 40.60 40.80 5000

45 Li 1 1 i ' 1 117 , ■ ■ 190 ■ 1 i ■ ■ " ■ i ' 219 1 I । '■ i ■ ■ । ■ । ■ 1 । 1 । । ' । ■ ' ' ' । ' ■ ■ ■ । ' 1 - ■ । 1 ■ ■■ । 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim ' l ' 1 1 1 I ' ' 73 40.20 40.40 40.60 40.80

I. m/z 355.10 20.92% 5000 147

221 281 397 A4E I I. i , 415 519 561 1 । ' 1 1 1 । ' ■ ' ■ । ■ ' 1 1 । । ' ■ ' t । । ” 1 । । ' । 1 । ' । । । । 1 1 ' ' । ' 1 । ' । । ■' ' 1 । ' ' i i i i [ i i I D I । । । । i II j । i t i r m/z—> 50 100 150 200 250 300 350 400 450 500 550 40.20 40.40 40.60 40.80

10432.D GCMS0510.M Thu May 16 10:20:30 2002 Page 5

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