GCMS unknowns report for sample AE02561, March 2002

Machine-extracted title · confidence 90%

Laboratory report detailing analysis of unknown compounds and surrogate recovery for sample AE02561.

NYC-WTC_000038784–000038800

Folder label: “GCMS X 3/4/02 A 3/20/02”

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NYC 9/11 Public Portal Document DCCLUlL ~pulIU LCDUL

Data File : C:\HPCHEM\l\DATA\MAR1902\2561.D Vial: 20 Acq On : 20 Mar 2002 11:43 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 9 Silanamine, N-[2,6-dimethyl-4- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

38.85 0.62 ug/1 61517 Perylene-dl2 37.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Silanamine, N-12,6-dimethyl-4 -[(tri 281 C14H27NOSi2 072088-09-6 10 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 10 3 Trisiloxane,/ 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 9 4 Tris (trimetkylsilyl) borate 278 C9H27BO3S13 004325-85-3 9 Abundance. Scan 3683 (38.855 min): 2561.D (-) ' m/ z 73.00.... 100.00% 73 147 5000 221 231 355

J .0 429 44 TH 91 — 1931 253 1’Tun 327 In'1 p1 f • I l 11 I I I • 1 1 I I 11 i'"11' ■'11 _____38.60 38.80 39.00 39.20__ m/ Z 1 47.00 63.2 5 % m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #39584: Silanamine, N-[2,6-dimethyl-4-[(trimethylsilyl)oxy] 713 281 209 MA MMAAR , — 5000 45 251 38.60 38.80 39.00 39.20 .. 179 125 147 1 T—T] 1 "I _........................................... i | I i > I ] 1 I I q r. 1 1 p rFT| . H i j i ( i r | ih i | i i 1 i I i i ■ 1 ] i b i I |

m/x->___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance 73 ----------------A-----

X 38.60 38.80 39.00 39.20 5000 355 45 133 193 223 281 TLUTTTTTTTTTTTTTTTTTTTTTTTTTTTTTUTTTEUTTTTTTTTTTTTTT

.... Ar“n TrpTTTYrrrTp-rTTpTTTyrTTTpTr^^ miz-2 40 60 80 100 120140 160180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #52459: Trisiloxane, 1,1,1,5,5.5-hexamethyl-3.3-bis[(trimet ' 1 1 1 1 1 1 1 1 I 1 1 1 ' I ' t ' ' i 1 ■ 73 147 38.60 38.80 39.00 39.20__

281 m/z 281.00 31.44% 5000

369 wMoM WWM- 207 249 । I 338 "ITIIUTTTTTT TT i1 n ■ । ' T '"i n-rj-rm-j- II 1'11 • i''" i mlz- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 38.60 38.80 39.00 39.20

2561.D GCMS0308.M Thu Mar 21 14:17:58 2002 Page 9

NYC-WTC_000038799

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