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GCMS analysis results for sample AE01462, Mar 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis report for environmental sample AE01462 dated March 29, 2002.

NYC-WTC_000038632–000038641

Folder label: “GCMS X 2/25/02 A 3/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\1462.D Vial: 42 Acq On : 24 Mar 2002 10:33 am Operator: Sample : re-extract Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 3-Quinolinecarbonitrile, 1,2,3 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.21 ug/1 36833 Phenanthrene-dl0 25.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Quinolinecarbonitrile, 1, 2,3,4-te 188 C10H8N2O2 022384-05-0 47 2 Cyclohexanone ,/phenylhydrazone 188 C12H16N2 000946-82-7 45 3 5-Methyl-2-p' nyl-2-hexenal 188 C13H16O 021834-92-4 43 4 Antipyrine / 188 C11H12N2O 000060-80-0 Abundance Scan 2261 (25.799 min):1462.D (-) m/z 188.10 100 .00 % 40

5000 - . .............------................. 94 160 40 54 80 114 — 1111111> 11111' 1111 > ।' 25.40 25.60 25.80 26.00 26.20 TP........ . l| ■■■■ m/z 187.20 26.21% m/z->.. 30 . 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #1 9815: 3-Quinolinecarbonitrile, 1,2,3,4-tetrahydro-1 -hydro 188

128 172 93 5000 117 1 142 25.40 25.60 25.80 26.00 26.20 66 m/z 189.05 14.91% - —ImTTT miz- 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180190 Abundance 188 93 i 1 ■ • 1 r ‘ 1 ^Tl i । । । 1 ‘ • i ' ' 25.40 25.60 25.80 26.00 26.20 5000 m/z 94.00 14.78% 65 77 106 120 132 145 159 170 i ■r 1 ■ । 1111 < 1 I I 1 1 I j ■ ■ I I I l t i ■ I I I I TT 11111111111 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69187: 5-Methyl-2-phenyl-2-hexenai 25.40 25.60 25.80 26.00 26'20 188 117 m/ z 18 . 10 11.70%

5000- 104 132 145 173 ............................. 1 1' I'1 ’ ■ I' ■'11'11' 1111111'1 TT’s "111 — ' i • ■ ■1111111111111' I’’ m/z~> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

1462.D GCMS0308.M Tue Mar 26 10:41:05 2002 Page 2

NYC-WTC_000038640

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NYC-WTC_000038640Source: NYC Law Department, mirrored locally

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