GCMS analysis results for sample AE03834, Mar 18 2002

NYC 9/11 Public Portal Document Library searen compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\3834.D Vial: 74 Acq On : 24 Feb 2002 6:51 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Butanamide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

9.26 1.51 ug/1 107623 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanamide / 87 C4H9NO 000541-35-5 64 2 3-Hydroxy>3-methyl-2-butanone 102 C5H10O2 000115-22-0 59 3 3-Pentanpl 88 C5H120 000584-02-1 40 4 Amylene Hydrate (r 88 C5H120 ________ 000075-85-4 38 'Abundance / Scan 460 (9.21 min): 3834.D (-) m/z 59.05 100.00% i 59

5000

■ ■ i ' 1 TII—nr—m 153 9.00 9.20 9.40 9.60 , 88 87 11....... " I '■'■'■i (। ' 11 |' । ’' |' 107 i1''' i T'' ‘ ' I T 11 i 1 1 ■ 1 i ■ m/ z 43 . . 41.02% m/z-> 10 20 30 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62880: Butanamide 44 59

5000 2 9.00 9.20 9.40 9.60 72 m/ z 41.05 18.29% | 87 m/z-> Abundance 10 20 30 40 150780 ■ i > ■ ■ • । 70 80 • i ■ 90 100 110 120 130 140 150 160 #63477: 3-Hydroxy-3-methyl-2-butanone I ' * ' ' I i ■ • ■ • i1" • i ■ ■ ■ ■ r

i I 59 - I 9.00 9.20 9.40 9.60 5000 31 V m/z 69.0,0 9.06% 43

15 । 69 87 102 ' I ’ 1 ’ ' I ' '' ‘ f ' •1 11 ' i ■ ■ ■ ■ i • < ■ ■ i ■ ■ ■ ■ i > । 1 ■ । ■1 1 > I T‘ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #851: 3-Pentanol 59 9.00 9.20 9.40 9.60 I m/z 152.90 6.87% 31 5000 41 15 ■ • i • • ■ ■ i ■ TT T TTT I ■ ■ 1 1 । ■ 1 ■ 1 । 1 ■ ■ ' । ■ 1 ' 1 । • 1 ■ । 1 ' ■ ■ । 1 ■ ■ ■ । ' 1 । 1 1 1 1 । 1 1 1 1 । '. m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.00 9.20 9.40 9.60

3834.D GCMS0208.M Wed Mar 13 11:34:01 2002 Page 3

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