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GCMS analysis results for sample AE03834, Mar 18 2002

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Laboratory report documenting GCMS analysis of sample AE03834 for unknown compounds on March 18, 2002.

NYC-WTC_000038364–000038374

Folder label: “GCMS X 2/22/02 A 2/24/02

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Scanned page image, NYC-WTC_000038371
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NYC 9/11 Public Portal Document Library searen compound Keporc

Data File : C:\HPCHEM\l\DATA\FEB2102\3834.D Vial: 74 Acq On : 24 Feb 2002 6:51 pm Operator: Sample : gc/ms scan 2/22 Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L.

Peak Number 2 N-Acetylpyrrolidone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

8.35 0.30 ug/1 21218 1,4-Dichlorobenzene-d4 12.33

- Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 N-Acetylpyrrolidon 127 C6H9NO2 000932-17-2 25 2 Dotriacontane .451 C32H66 000544-85-4 9 3 2-Propanone-; 1-trichloro- 160 C3H3C13O 000918-00-3 9 4 Heptacosane 380 C27H56 000593-49-7 9 'Abundance • 7 Scan 361 (8.354 min): 3834.D (-) m/z 4,3.00 TOO. 00% i 4

5000

97 125 -----I T' -------IT 8.00 8.20 8.40 8.60 — Il || 1 m/z 124.95 12.77% m/z-> 50 100 150 200 • 250 300 350 400 450 'Abundance #4732: N-Acetylpyrrolidone 43

5000 r .......... 8.00 8.20 8.40 8.60_____ 99 127 m/z 41.95 9.33% — 69,1 , I ' m/z-> 50 100 150 200 250 300 350 400 450 Abundance #74490; Dotriacontane 43; TT i l 71 8.00 8.20 8.40 8.60 5000 m/ Z 96.95 8.91% I : । ' 97 ' l ! :,0127,155183 ..... •...... 379 407 450 miz-> 50 100 150 200 250 300 350 400 450 'Abundance #12247: 2-Propanone, 1,1,1-trichloro- TT 43 8.00 8.20 8.40 8.60 m/ z 8.07% 46 ’ 85 5000 -

15 I 85 125 ... — TT m/z-> 50 100 150 200 250 300 350 400 450 8.00 8.20 8.40 8.60

3834.D GCMS0208.M Wed Mar 13 11:33:56 2002 Page 2

NYC-WTC_000038371

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NYC-WTC_000038371Source: NYC Law Department, mirrored locally

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