GCMS analysis results for unknown compounds, June 2002

NYC 9/11 Public Portal Document ubrary searen compound Keporc

Data File C:\MSDCHEM\1\DATA\060702\12738.D Vial: 14 Acq On 7 Jun 2002 7:10 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Piperidine, 2-propyl-, (S)- Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 4.36 1.25 ug/L 727930 1,4-dichlorobenzene-d4 9.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Piperidine, 2-propyl-, (S)- 127 C8H17N 000458-88-8 1/ 2 Borane, trifluoro- 68 BF3 007637-07-2 1 3 2-Chloroethanol 80 C2H5C1O 000107-07-31 4 2-Chioroethanol 80 C2H5C1O 000107-07/3 1 Abundance Scan 218 (4.360 min): 12738.D (-217) (-) m/z 49.10 100.00% 49 84

5000

41 400 4.20 4.40 4.60 4.80 0- - lyui n ' — m/z 84.00 78.31% miz-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #33701: Piperidine, 2-propyl-, (S)- 84

5000 400 4.20 4.40 4.60 4.80 m/z 47.10 29.89% 56 0- ,1 69 ■111' ■ ■ i ■ ■ • ■ i ■ ■1111111 r 111 11'1 '‘‘T111111 ! TTTT+98 127 —WIIP /z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12321: Borane, trifluoro- 49 400 4.20 4.40 4.60 4.80 5000 m/z 41.05 20.30%

n/z-> 11 19 0-—— O 0 10 20 30 38 30 40 50 68

60 70 80 90 100 110 120 130 "MWAV/u Abundance #108293:2-Chloroethanol 31 400 4.20 4.40 4.60 4.80 m/z 42.05 11.51% 5000 ""MWMMas 0- ......... I 1— 37 43mp ' ' ) 1 ‘ ‘I * * ’ 49 61 80 1 11 1 1 T"7 111 । । > । । 1111 n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 4.00 4.20 4.40 4.60 4.80

12738.D 060302.M Mon Jun 10 11:45:37 2002 Page 11

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