GCMS quantitation report, May 22 2002

NYC 9/11 Public Portal Document ulbrary searcn compound Keporc

Data File : C:\MSDCHEM\1\DATA\052202\11905.D Vial: 12 Acq On : 22 May 2002 10:47 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan ' *= Library : C:\DATABASE\NIST98.L

Peak Number 2 Propiolonitrile Concentration Rank 9

R.T. EstConc Area Relative to, ISTD R.T. 3.73 0.34 ug/L 259429 1 ,4-Dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Propiolonitrile 51 C3HN 001070-71-9 3 2 Ethyl Chloride 64 C2H5C1 000075-00-3/2 3 2-Chloroethanol 80 C2H5C10 000107-07-3 2 4 2-p-Nitrobenzoyl-l,3,5-tribenzyl... 569 C33H31NO8 1000129-85-6 1 Abundance Scan 110 (3.726 min): 11905.D (-109) (-) m/z 51.10 100.00% 51

5000 82 86 4447 35 40 58 | i i p | 11 p 1 i i p m p i , , ।, 1 . . । . # - . . । , 3.40 3.60 3.80 4.00 o+1‘I‘1111$1—30000100101TTTTI1-" 1‘ ‘ F TIT m/z 49.10 63.18% mlz~> 5 10 15 20253035404550556065 70 75 80859095 Abundance #12371: Propiolonitrile 51

5000 3.40 3.60 3.80 4.00 m/z 86.00 45.66% /. m/z-> Ot 5 +12,18,428,32. 38+++47. 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #107943: Ethyl Chloride 23 ’ ’1***I**’IIII17II! 3.40 3.60 3.80 4.00 64 5000 m/z 82.00 39.77% 49 25 35 67, 111111..ii1111111.111111.11 Ot 1215 TH TTHT ............. I,I..... miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1032:2-Chloroethanol i ■ • ■ ■ I 31 3.40 3.60 3.80 4.00 m/z 47.10 38.46%

5000 /MIula 43 . 0 12, 18 2427) ■i । P11111111111 ii 111111 *]] 3538 ,1 49,53 586164 76 80 n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■ ■ i ■ ■ ■ ■ i ■ 1 ■ ' i ■ ■ ■ ■ i ■ ■ ■ ■ i 3.40 3.60 3.80 4.00

11905.D 052202.M Tue May 28 12:11:58 2002 Page 5

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