GCMS analysis results for sample AD31591, Feb 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report 3

Data File : C:\HPCHEM\l\DATA\FEB2102\31591.D Vial: 38 Acq On : 23 Feb 2002 3:36 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1-Eicosanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.31 0.92 ug/1 72526 Chrysene-dl2 33.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Eicosanol / 298 C20H42O 000629-96-9 76 2 1-Octadecanol 270 C18H380 000112-92-5 76 3 1-Docosene / 308 C22H44 001599-67-3 68 4 Phosphonic acid, dioctadecyl ester 587 C36H75O3P 019047-85-9 68 Abundance Scan 2861 (31.311 min): 31591. D (-) m/ z 55.0,0 100 . 00% 55

5000 4 73 97 in 127 TI

m/z-> 40 —l—plL 60 . .... - 80 100 -120 140 160 180 200 220 240 260 280 300 m/z 31.00 31.20 31.40 31.60 43.00 57.19% 'Abundance #72723: 1-Eicosanol 43 $7 83 97 5000 70 111 31.00 31.20 31.40 31.60 125 _ m/z 57.00 46.22% r ■ i ■ T ■ • i • 1 — 1139 ............ ,252, _ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72029: 1-Octadecanol 43 57 83 . 97 31.00 31.20 31.40 31.60 5000- 70 m/z 73.0,0 44.65% 111 i j 125 i 1. 224 252 ' I ' 1 ' 1 I ' ' 1 1 I 1 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72943: 1-Docosene • > i ■ ■ • ■ i ■ ■ ■ । ■ ■ ■ ■ । • ■ • ■ । 55 31.00 31.20 31.40 31.60 83 97 m/z 83.0,5 40.18% 5000 - 70 111 42

miz—> ■ ' i ■ ■ 40 60 80 H 100 120 125 139 308 "‘OIE111"EEIT‘IEIO1E"T—TET"TLIIEIIIIIIIITIT 140 160 180 200 220 24C 260 280 300 MAAAN 31.00 31.20 31.40 31.60

31591.D GCMS0208.M Wed Feb 27 12:06:16 2002 Page 4 NYC-WTC_000038215