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GCMS analysis results for sample AE03801, March 22, 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03801 conducted on March 22, 2002.

NYC-WTC_000037906–000037926

Folder label: “GCMS X 2/20/02 A 3/20/02

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NYC 9/11 Public Portal Document

i LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\031902\3801.D Vial: 11 Acq On : 19 Mar 2002 7:51 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 8.908 638 643 649 rBV 98675 206063 2.04% 0.338% 2 9.543 708 713 733 rBV 2319003 6707289 66.25% 11.008% 3 12.046 985 989 1005 rBV 439459 825886 8.16% 1.355% 4 13.026 1091 1097 1122 rBV 4311488 9406785 92.92% 15.439% 5 15.112 1322 1327 1339 rBV 741478 1336124 13.20% 2.193% 6 15.956 1415 1420 1426 rBV 65340 132989 1.31% 0.218% 7 17.842 1623 1628 1642 rVB 490174 940701 9.29% 1.544% 8 18.133 1654 1660 1681 rBV 4844354 10071938 99.49% 16.531% 9 18.768 1726 1730 1740 rBV 72339 214758 2.12% 0.352% 10 20.282 1892 1897 1905 rBV 375181 700004 6.91% 1.149% 11 22.387 2124 2129 2135 rBV2 287945 525760 5.19% 0.863% 12 22.495 2135 2141 2155 rW2 4551477 10123553 100.00% 16.615% 13 22.650 2155 2158 2167 rVB3 35844 122144 1.21% 0.200% 14 24.264 2330 2336 2344 rBB 197447 368514 3.64% 0.605% 15 25.969 2519 2524 2531 rBB 146552 290978 2.87% 0.478% 16 27.430 2680 2685 2691 rBV 899786 1765244 17.44% 2.897% 17 27.529 2691 2696 2705 rVB 149045 349735 3.45% 0.574% 18 28.962 2848 2854 2865 rBB 114664 242795 2.40% 0.398% 19 30.305 2995 3002 3029 rBV2 4053530 10042010 99.19% 16.482% ' 20 30.913 3063 3069 3082 rVB 94304 236897 2.34% 0.389% 21 31.593 3138 3144 3155 rBV2 84561 212990 2.10% 0.350% 22 32.790 3268 3276 3288 rBV 63218 165221 1.63% 0.271% 23 33.906 3392 3399 3407 rBV 46524 119279 1.18% 0.196% 24 34.178 3422 3429 3447 rBV2 2340801 5821306 57.50% 9,. 554%

Sum of corrected areas: 60928963

3801.D 5080302.M Thu Mar 21 11:43:36 2002 Page 1

NYC-WTC_000037911

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