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GCMS analysis report, sample AE02339, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02339 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010610–000010630

Folder label: “GCMS X 1/31/02 A 3/4/02

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Scanned page image, NYC-WTC_000010615
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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\030402\2339.D Vial: 11 Acq On 4 Mar 2002 6:27 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 8.935 640 646 652 rBV 100591 191130 1.93% 0.314% 2 9.579 711 717 729 rBV 2806663 6831106 69.01% 11.213% 3 12.074 988 992 1002 rVB2 530653 917741 9.27% 1.506% 4 13.053 1094 1100 1114 rBV 4793152 9012958 91.05% 14.794% 5 15.140 1325 1330 1340 rVB 903967 1479910 14.95% 2.429%

6 15.983 1419 1423 1432 rBV 86739 154977 1.57% 0.254% 7 17.870 1627 1631 1638 rVB 643464 1125954 11.38% 1.848% 8 18.169 1657 1664 1677 rBV 4871054 9793422 98.94% 16.075% 9 18.795 1729 1733 1742 rBV 99745 186531 1.88% 0.306% 10 20.310 1895 1900 1905 rBV 502397 839604 8.48% 1.378%

11 22.414 2127 2132 2137 rBV2 385889 672611 6.80% 1.104% 12 22.523 2137 2144 2157 rBV2 4446712 9898432 100.00% 16.247% 13 24.291 2334 2339 2345 rBB 278506 502893 5.08% 0.825% 14 25.997 2522 2527 2533 rBB 235397 438256 4.43% 0.719% 15 27.457 2684 2688 2694 rBV 542944 970813 9.81% 1.593%

16 27.557 2694 2699 2707 rVB2 218739 448511 4.53% 0.736% 17 28.990 2851 2857 2869 rBV 190560 411731 4.16% 0.676% 18 30.341 2998 3006 3020 rBV2 4064117 9706436 98.06% 15.932% 19 31.620 3140 3147 3161 rBV2 129934 327919 3.31% 0.538% 20 32.817 3273 3279 3292 rBV 101339 252236 2.55% 0.414%

21 33.942 3397 3403 3408 rBV 67250 166495 1.68% 0.273% 22 34.214 3425 3433 3453 rBV2 2670549 6471346 65.38% 10.622% 23 34.985 3513 3518 3524 rBV2 45796 122528 1.24% 0.201%

Sum of corrected areas: 60923540

2339.D 5080302.M Mon Mar 18 08:32:35 2002 Page 1

NYC-WTC_000010615

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NYC-WTC_000010615Source: NYC Law Department, mirrored locally

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