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GCMS analysis report, sample AE02336, March 22, 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for sample AE02336 conducted on March 22, 2002, listing unknown compounds and surrogates.

NYC-WTC_000010558–000010576

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

: Data File C:\MSDCHEM\l\DATA\030402\2336.D Vial: 8 Acq On 4 Mar 2002 4:00 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 8.935 642 646 653 rVB 60013 115820 1.17% 0.198% 2 9.579 711 717 737 rBV 2772199 7000167 70.53% 11.995% 3 12.074 988 992 1001 rVB 287230 492815 4.97% 0.844% 4 13.053 1094 1100 1115 rBV 4851944 9089956 91.59% 15.575% 5 15.140 1325 1330 1337 rVB 561143 903793 9.11% 1.549% 6 17.870 1627 1631 1637 rVB 404216 693586 6.99% 1.188% 7 18.169 1657 1664 1675 rBV 4746609 9808650 98.83% 16.807% 8 18.795 1728 1733 1743 rBV 57065 113481 1.14% 0.194% 9 20.310 1895 1900 1906 rBB 305642 510907 5.15% 0.875% 10 22.414 2127 2132 2138 rBV 238509 411022 4.14% 0.704% 11 22.523 2138 2144 2158 rBV2 4471949 9924859 100.00% 17.006% 12 24.291 2334 2339 2343 rBV 173875 301437 3.04% 0.517% 13 25.997 2522 2527 2532 rBB 141171 268587 2.71% 0.460% 14 27.457 2683 2688 2694 rBV 592404 1073990 10.82% 1.840% 15 27.557 2694 2699 2705 rVB2 142030 282895 2.85% 0.485% 16 28.990 2851 2857 2865 rBV 123845 255838 2.58% 0.438% 17 30.341 2997 3006 3029 rBV2 4099652 9667456 97.41% 16.565% 18 31.620 3142 3147 3155 rBV2 81087 202863 2.04% 0.348% 19 32.817 3272 3279 3294 rBV2 58348 159515 1.61% 0.273% 20 33.942 3397 3403 3414 rBV 44978 115249 1.16% 0.197% 21 34.214 3426 3433 3450 rBV2 2844037 6968090 70.21% 11.940%

Sum of corrected areas: 58360976

2336.D 5080302.M Mon Mar 18 08:31:39 2002 Page 1

NYC-WTC_000010563

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NYC-WTC_000010563Source: NYC Law Department, mirrored locally

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