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GCMS blank analysis results for sample AE03265, March 2002

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Laboratory report documenting GCMS blank analysis of environmental sample AE03265 conducted on March 25, 2002.

NYC-WTC_000011347–000011364

Folder label: “GCMS X 2/14/02 A 3/2/02 - 3/20/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\031902\0214LB.D Vial: 33 Acq On : 21 Mar 2002 5:58 am Operator: McLean Sample : 2/14/02 RE-INJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) . Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.561 270 274 297 rBV 625371 1833317 7.64% 1.339% 2 9.552 708 714 734 rBV 6809543 16543136 68.90% 12.085% 3 12.056 985 990 1001 rBV 424759 748627 3.12% 0.547% 4 13.035 1091 1098 1112 rBV 10433717 22057719 91.87% 16.113% 5 15.112 1322 1327 1338 rBV 1011617 1849616 7.70% 1.351%

6 15.956 1416 1420 1425 rBV 145880 276849 1.15% 0.202% 7 17.852 1624 1629 1641 rBV 844863 1524384 6.35% 1.114% 8 18.151 1654 1662 1666 rBV 10012555 23282030 96.96% 17.008% 9 18.777 1727 1731 1746 rBV 145596 397209 1.65% 0.290% 10 20.291 1892 1898 1907 rBB 616032 1202494 5.01% 0.878%

11 22.396 2124 2130 2135 rBV2 486712 970014 4.04% 0.709% 12 22.523 2135 2144 2155 rBV2 8919099 24010848 100.00% 17.540% 13 24.264 2331 2336 2347 rBB 391998 727692 3.03% 0.532% 14 25.978 2519 2525 2534 rBB 314503 640154 2.67% 0.468% 15 27.430 2681 2685 2692 rBV 941098 1946593 8.11% 1.422%

16 27.529 2692 2696 2704 rVB2 307320 683674 2.85% 0.499% 17 28.963 2849 2854 2866 rBV2 247275 621384 2.59% 0.454% 18 30.332 2996 3005 3029 rBV2 7517817 22566553 93.98% 16.485% 19 31.602 3136 3145 3156 rBV2 170438 498705 2.08% 0.364% 20 32.790 3270 3276 3286 rBV2 118025 359727 1.50% 0.263%

21 34.205 3423 3432 3453 rBV2 4890203 14150678 58.93% 10.337%

Sum of corrected areas: 136891403

0214LB.D 5080302.M Mon Mar 25 08:59:10 2002 Page 1

NYC-WTC_000011352

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NYC-WTC_000011352Source: NYC Law Department, mirrored locally

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