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GCMS analysis results for sample AE03804, March 22, 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03804 conducted on March 22, 2002.

NYC-WTC_000037948–000037963

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037953
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\031902\3804.D Vial: 14 Acq On : 19 Mar 2002 10:18 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multipir: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 8.908 638 643 649 rBV 75569 159124 1.72% 0.306% 2 9.543 709 713 734 rBV 2105583 5911236 63.81% 11.376% 3 12.047 984 989 1000 rBV 308380 563583 6.08% 1.085% 4 13.017 1091 1096 1113 rBV 3812007 8289488 89.48% 15.953% 5 15.112 1322 1327 1337 rBV 462986 818756 8.84% 1.576%

6 15.956 1415 1420 1424 rBV 54305 102569 1.11% 0.197% 7 17.842 1623 1628 1636 rBV 324459 588085 6.35% 1.132% 8 18.133 1654 1660 1684 rBV 4534406 9200004 99.31% 17.705% 9 18.777 1727 1731 1736 rBV 46448 109309 1.18% 0.210% 10 20.282 1892 1897 1906 rVB 233641 427084 4.61% 0.322%

11 22.387 2124 2129 2134 rBV 173725 314000 3.39% 0.604% 12 22.495 2134 2141 2155 rBV2 4162497 9263956 100.00% 17.828% 13 22.650 2155 2158 2166 rVB2 33745 106911 1.15% 0.206% 14 24.264 2331 2336 2342 rBB 115414 223890 2.42% 0.431% 15 25.969 2519 2524 2532 rBB 89661 175604 1.90% 0.338%

16 27.430 2680 2685 2691 rBV 846689 1605036 17.33% 3.089% 17 27.520 2691 2695 2703 rVB2 84369 191765 2.07% 0.369% 18 28.963 2849 2854 2860 rBV2 61905 132165 1.43% 0.254% 19 30.305 2995 3002 3031 rBV2 3778511 8857317 95.61% 17.046% ' 20 31.593 3138 3144 3153 rBV2 41634 101335 1.09% 0.195%

21 34.178 3422 3429 3453 rBV 1946477 4820339 52.03% 9.277%

Sum of corrected areas: 51961556

3804.D 5080302.M Thu Mar 21 11:48:01 2002 Page 1

NYC-WTC_000037953

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NYC-WTC_000037953Source: NYC Law Department, mirrored locally

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