GCMS analysis results for sample AE03803, March 22, 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\031902\3803.D Vial: 13 Acq On : 19 Mar 2002 9:29 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 8.908 639 643 648 rBV 68884 144801 1.51% 0.281% 2 9.543 708 713 741 rBV 2159140 6239698 65.04% 12.093% 3 9.833 741 745 760 rVB4 23302 101770 1.06% 0.197% 4 12.047 985 989 998 rBV 228458 411456 4.29% 0.797% 5 13.026 1091 1097 1113 rBV 3924216 8575087 89.38% 16.619%

6 15.112 1321 1327 1338 rBV2 299124 543336 5.66% 1.053% 7 17.843 1624 1628 1635 rBV2 193628 353664 3.69% 0.685% 8 18.133 1654 1660 1680 rBV 4625649 9436308 98.36% 18.288% 9 20.282 1892 1897 1904 rBB 136240 250663 2.61% 0.486% 10 22.387 2123 2129 2134 rBV2 103713 186267 1.94% 0.361%

11 22.496 2134 2141 2155 rBV2 4254081 9593589 100.00% 18.593% 12 22.650 2155 2158 2166 rVB2 35149 103657 1.08% 0.201% 13 24.264 2331 2336 2341 rBB 64989 125199 1.31% 0.243% 14 25.969 2519 2524 2530 rBB2 52932 99259 1.03% 0.192% 15 27.430 2680 2685 2692 rBV 790352 1525042 15.90% 2.956%

16 27.530 2692 2696 2701 rVB2 46403 98864 1.03% 0.192% 17 30.305 2995 3002 3025 rBV2 3774438 8852112 92.27% 17.156% 18 34.178 3422 3429 3450 rBV 1979607 4956730 51.67% 9.607%

Sum of corrected areas: 51597502

3803.D 5080302.M Thu Mar 21 11:46:02 2002 Page 1

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