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GCMS re-injection results, Sample 1639, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report for GC/MS re-injection of sample 1639 using Method 508 scan on March 20-21, 2002.

NYC-WTC_000012129–000012144

Folder label: “GCMS X 3-1-02 A 3-20-02 MANY RERNNS

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Scanned page image, NYC-WTC_000012134
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NYC 9/11 Public Portal Document

LSC Area Percent Report

.. Data File : C:\MSDCHEM\1\DATA\031902\1640.D Vial: 25 Acq On : 20 Mar 2002 10:32 am Operator: McLean Sample : RE-INJ 3/1 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.543 708 713 733 rBV 1847944 5288854 63.43% 11.343% 2 9.833 741 745 758 rVB5 25035 99346 1.19% 0.213% 3 12.046 985 989 998 rBV 214446 383709 4.60% 0.823% 4 13.017 1091 1096 1112 rBV 3370350 7428996 89.10% 15.934% 5 15.112 1322 1327 1335 rBV 409929 723724 8.68% 1.552%

6 17.842 1624 1628 1638 rBV 271582 535649 6.42% 1.149% 7 18.132 1654 1660 1683 rBV 4028375 8255827 99.02% 17.707% 8 20.282 1892 1897 1906 rBV 205110 394940 4.74% 0.847% 9 22.386 2124 2129 2135 rBV 153500 288760 3.46% 0.619% 10 22.495 2135 2141 2154 rBV2 3589383 8337715 100.00% 17.883%

11 24.264 2331 2336 2344 rBB 109316 207019 2.48% 0.444% 12 25.978 2517 2525 2526 rBV 98480 182189 2.19% 0.391% 13 27.429 2680 2685 2692 rBV 719970 1480796 17.76% 3.176% 14 27.529 2692 2696 2706 rVB 81498 189688 2.28% 0.407% 15 28.962 2849 2854 2866 rBB2 57102 138436 1.66% 0.297%

16 30.305 2995 3002 3020 rBV2 3346081 8017407 96.16% 17.196% 17 31.593 3139 3144 3155 rBV 44234 108092 1.30% 0.232% 18 34.178 3422 3429 3450 rBV2 1814659 4563504 54.73% 9.788%

Sum of corrected areas: 46624651

1640.D 5080302.M Thu Mar 21 06:31:20 2002 Page 1

NYC-WTC_000012134

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