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GCMS blank results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.

NYC-WTC_000037848–000037869

Folder label: “GCMS X 2/20/02 A 3/20/02

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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

0 = LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\031902\220LB.D Vial: 8 Acq On : 19 Mar 2002 5:24 pm Operator: McLean Sample : RE-INS 2/20 Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total --- ----- ----- ---- ---- --- ------- 1 8.908 639 643 652 rBV 120154 254484 2.19% 0.331% 2 9.543 708 713 735 rBV 2605691 7483078 64.27% 9.723% 3 12.047 985 989 1003 rBV 715410 1353797 11.63% 1.759% 4 13.026 1091 1097 1113 rBV 5088937 10425951 89.55% 13.547% 5 15.112 1322 1327 1337 rBV 1486023 2589700 22.24% 3.365%

6 15.956 1416 1420 1432 rBV 145897 292059 2.51% 0.379% 7 17.842 1623 1628 1643 rVB 1188280 2293476 19.70% 2.980% 8 18.133 1654 1660 1683 rBV 5328663 11460613 98.43% 14.891% 9 18.768 1726 1730 1749 rBV 280770 786733 6.76% 1.022% 10 20.282 1892 1897 1908 rBV 938605 1730377 14.86% 2.248%

11 22.387 2124 2129 2135 rBV2 700252 1323679 11.37% 1.720% 12 22.495 2135 2141 2154 rVV2 5187741 11557112 99.26% 15.016% 13 22.650 2155 2158 2172 rVB2 43781 170912 1.47% 0.222% 14 24.264 2330 2336 2344 rBV 493238 964330 8.28% 1.253% 15 25.969 2519 2524 2532 rBV 381826 798184 6.86% 1.037%

16 27.430 2680 2685 2691 rBV 1149689 2180167 18.72% 2.833% 17 27.529 2691 2696 2706 rVB2 352256 835152 7.17% 1.085% 18 28.963 2848 2854 2866 rBV2 282296 721730 6.20% 0.938% 19 30.314 2995 3003 3029 rBV 4676721 11643191 100.00% 15.128% 20 30.913 3063 3069 3081 rBV 100598 258784 2.22% 0.336%

21 31.593 3138 3144 3161 rBV 182205 556551 4.78% 0.723% 22 32.790 3268 3276 3290 rBV 132991 395880 3.40% 0.514% 23 33.906 3392 3399 3414 rBV2 93388 273893 2.35% 0.356% 24 34.178 3422 3429 3446 rBV2 2522377 6440726 55.32% 8.369% 25 34.958 3509 3515 3522 rBV3 62175 172933 1.49% 0.225%

Sum of corrected areas: 76963492

220LB.D 5080302.M Thu Mar 21 11:52:28 2002 Page 1

NYC-WTC 000037852

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NYC-WTC_000037852Source: NYC Law Department, mirrored locally

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