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GCMS analysis results for sample AE03805, March 22, 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03805 conducted on March 22, 2002.

NYC-WTC_000037964–000037977

Folder label: “GCMS X 2/20/02 A 3/20/02

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NYC 9/11 Public Portal Document

« LSC Area Percent Report

Data File : C:\MSDCHEM\1\DATA\031902\3805.D Vial: 15 Acq On : 19 Mar 2002 11:07 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation-: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 8.908 639 643 651 rBV 75057 152952 1.58% 0.281% 2 9.543 708 713 733 rBV 2261897 6291502 64.94% 11.578% 3 12.046 985 989 1000 rBV 265514 493651 5.10% 0.908% 4 13.026 1091 1097 1118 rBV 4098988 8822054 91.06% 16.235% 5 15.112 1322 1327 1338 rBV 454618 806015 8.32% 1.483%

6 17.851 1624 1629 1639 rBV 334487 637961 6.58% 1.174% 7 18.133 1654 1660 1679 rBV 4668189 9678602 99.90% 17.811% 8 18.777 1727 1731 1739 rBV2 41629 125400 1.29% 0.231% 9 20.282 1892 1897 1905 rBV 242103 441652 4.56% 0.813% 10 22.387 2124 2129 2135 rBV2 157968 296071 3.06% 0.545% 11 22.495 2135 2141 2155 rW2 4250953 9688281 100.00% 17.829% 12 22.650 2156 2158 2171 rVB3 36469 118382 1.22% 0.218% 13 24.264 2331 2336 2342 rVB 96006 179843 1.86% 0.331% 14 25.969 2519 2524 2531 rBB2 63279 124870 1.29% 0.230% 15 27.430 2680 2685 2692 rBV 893989 1711758 17.67% 3.150% 16 27.520 2692 2695 2702 rVB 67199 144271 1.49% 0.265% 17 28.962 2849 2854 2861 rBV2 46251 98724 1.02% 0.182% 18 30.305 2995 3002 3029 rBV2 3861839 8976279 92.65% 16.519% 19 30.913 3064 3069 3079 rBV 121395 279685 2.89% 0.515% 20 34.178 3422 3429 3450 rBV2 2057742 5271462 54.41% 9.701%

Sum of corrected areas: 54339415

3805.D 5080302.M Thu Mar 21 11:49:00 2002 Page 1

NYC-WTC_000037969

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NYC-WTC_000037969Source: NYC Law Department, mirrored locally

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