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GCMS analysis results for sample AE02381, March 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of environmental sample AE02381 conducted on March 22, 2002.

NYC-WTC_000010659–000010676

Folder label: “GCMS X 1/31/02 A 3/4/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\030402\2381.D Vial: 16 Acq On 4 Mar 2002 10:32 pm Operator: McLean Sample 1/31 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.579 711 717 734 rBV 2532243 6327561 69.28% 11.977% 2 12.074 988 992 997 rVB 276581 464954 5.09% 0.880% 3 13.053 1094 1100 1115 rBV 4452809 8314607 91.04% 15.739% 4 15.140 1325 1330 1337 rVB2 511123 822933 9.01% 1.558% 5 17.870 1626 1631 1636 rBB 351772 606414 6.64% 1.148%

6 18.160 1657 1663 1676 rBV 4352637 9111458 99.77% 17.247% 7 18.795 1730 1733 1740 rBV 74573 135364 1.48% 0.256% 8 20.310 1895 1900 1905 rBV 282508 463608 5.08% 0.878% 9 22.414 2127 2132 2137 rBB2 203753 361098 3.95% 0.684% 10 22.523 2137 2144 2158 rBV2 4284060 9132777 100.00% 17.287%

•11 24.291 2334 2339 2344 rBV 151257 259977 2.85% 0.492% 12 25.997 2523 2527 2534 rBB 119367 221262 2.42% 0.419% 13 27.457 2684 2688 2694 rBV 517651 927008 10.15% 1.755% 14 27.557 2694 2699 2706 rVB 108016 220347 2.41% 0.417% 15 28.990 2852 2857 2865 rBV 89921 177622 1.94% 0.336%

16 30.341 2998 3006 3022 rBV2 3637024 8719334 95.47% 16.505% 17 31.620 3142 3147 3155 rBV 60632 135462 1.48% 0.256% 18 32.817 3273 3279 3289 rVB 43492 102896 1.13% 0.195% 19 33.398 3338 3343 3353 rBV 134535 319809 3.50% 0.605% 20 34.214 3425 3433 3454 rBV 2496231 6004925 65.75% 11.367%

Sum of corrected areas: 52829416

2381.D 5080302.M Mon Mar 18 08:33:15 2002 Page 1

NYC-WTC_000010664

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NYC-WTC_000010664Source: NYC Law Department, mirrored locally

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