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GCMS blank results for sample AE03799, March 22, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03799 to verify analytical system cleanliness.

NYC-WTC_000037848–000037869

Folder label: “GCMS X 2/20/02 A 3/20/02

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Scanned page image, NYC-WTC_000037856
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\031902\220LB.D Vial: 8 Acq On : 19 Mar 2002 5:24 pm Operator: McLean Sample : RE-INJ 2/20 Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L *********************************************************************

Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 15.11 4.97 ug/L 2589700 Naphthalene-d8 13.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual --------------------------------------------------------------------- 1 Cyclohexasiloxane, dodecamethyl-... 444 C12H36O6Si6 000540-97-6 94 2 Cyclohexasiloxane, dodecamethyl- 444 C12H36O6Si6 000540-97-6 91 3 5,6-exo-Epoxy-N-phenyl-l-trimeth... 341 C19H23NO3Si 000000-00-0 50 4 5-(2,3-BIS(TRIMETHYLSILYLOXY)PRO... 444 C20H40N2O5Si2 012774-38-8 33 undance Scan 1327 (15.112 min): 220LB.D (-) m/z 73.10 100.00

5000 341

147 429 45 14.80 15.00 15.20 15.40 0 117 179 207 251 281 311 397 m/z 341.00 38.24% -> 50 100 150 200 250 300 350 400 undance #352523: Cydohexasiloxane, dodecamethyl- $$ Dodecamethyic...

341

429 5000 14.80 15.00 15.2015.40 m/z 147.10 14.33 147 45 117 207 267 311 387 0 -> 50 100 150 200 250 300 350 400 undance #352522: Cyctohexasiioxane, dodecamethyl-

14.80 15.00 15.20 15.40 5000 m/z 429.10 13.15 341 429 147 0 45 117 177 207 237 271311 367 397 -> 50 100 150 200 250 300 350 400 undance #290888:5,6-exo-Epoxy-N-phenyl-1-trlmethylsilytmethylbicy... 14.80 15.00 15.2015.40 m/z 342.00 12.74

5000 326

-> 0 1. 4 1; . ' I ' ' ' ' l ' ' ' I ' ' ' ' I ' , ' l ' ' 50 100 150 200 250 300 - 350 I 400 14.80 15.00 15.20 15.40

9')AT.D Tt CAOA7A') UR 'Pt.... ER..... • " . . rn 1. - .'nn-' .. _ _ - ..

NYC-WTC 000037856

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NYC-WTC_000037856Source: NYC Law Department, mirrored locally

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