NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\031902\220LB.D Vial: 8
Acq On : 19 Mar 2002 5:24 pm Operator: McLean
Sample : RE-INJ 2/20 Inst : Instrumen
Misc Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator)
Title : Quantitation For Method 508gcscan
Library : C:\DATABASE\WILEY7N.L
*********************************************************************
Peak Number 3 Cyclohexasiloxane, dodecame... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
---------------------------------------------------------------------
15.11 4.97 ug/L 2589700 Naphthalene-d8 13.03
Hit# of 5 Tentative ID MW MolForm CAS# Qual
---------------------------------------------------------------------
1 Cyclohexasiloxane, dodecamethyl-... 444 C12H36O6Si6 000540-97-6 94
2 Cyclohexasiloxane, dodecamethyl- 444 C12H36O6Si6 000540-97-6 91
3 5,6-exo-Epoxy-N-phenyl-l-trimeth... 341 C19H23NO3Si 000000-00-0 50
4 5-(2,3-BIS(TRIMETHYLSILYLOXY)PRO... 444 C20H40N2O5Si2 012774-38-8 33
undance Scan 1327 (15.112 min): 220LB.D (-) m/z 73.10 100.00
5000
341
147 429
45 14.80 15.00 15.20 15.40
0
117 179 207 251 281 311 397 m/z 341.00 38.24%
-> 50 100 150 200 250 300 350 400
undance #352523: Cydohexasiloxane, dodecamethyl- $$ Dodecamethyic...
341
429
5000
14.80 15.00 15.2015.40
m/z 147.10 14.33
147
45 117 207 267 311 387
0
-> 50 100 150 200 250 300 350 400
undance #352522: Cyctohexasiioxane, dodecamethyl-
14.80 15.00 15.20 15.40
5000 m/z 429.10 13.15
341
429
147
0 45 117 177 207 237 271311 367 397
-> 50 100 150 200 250 300 350 400
undance #290888:5,6-exo-Epoxy-N-phenyl-1-trlmethylsilytmethylbicy...
14.80 15.00 15.2015.40
m/z 342.00 12.74
5000 326
->
0 1. 4 1; . ' I ' ' ' ' l ' ' ' I ' ' ' ' I ' , ' l ' '
50 100 150 200 250 300 - 350
I 400 14.80 15.00 15.20 15.40
9')AT.D Tt CAOA7A') UR 'Pt.... ER..... • " . . rn 1. - .'nn-' .. _ _ - ..
NYC-WTC 000037856
OCR can misread numbers and units. Confirm readings against the page image before using them.