GCMS analysis results for sample AE03617, March 28, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03617.D Vial: 7 Acq On : 8 Mar 2002 8:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-Buten-2-ol, 2-methyl­ Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

4.65 0.13 ug/L 72981 1,4-Dichl oroben zene - d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 12 2 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 12 3 2-Penten-l-ol, (Z) - $$ cis-2-Pen. . . 86 C5H10O 001576-95-0 9 4 2-Buten-l-ol, 3-methyl- (CAS) $$... 86 C5H10O 000556-82-1 9 Abundance Scan 113 (4.649 min): 03517.D (-) m/z 41.10 100.00% 41 71 88 57

5000 44 53 68 85 AAAAMMLA 49 4.40 4.60 4.80 5.00 0+ 1‘1111-1"-ET721-T TTIIT i • ■ *11 i “ “ i' ■' TI‘ th " ‘ ' T’rr m/z 71.00 93.23% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4084:3-Buten-2-ol, 2-methyl- 71 43

5000 A AA — 59 4.40 4.60 4.80 5.00 m/z 88.00 85.61% 27 53 67 86 01 —mmT HH —mp -HP miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4076:2-Buten-l-ol, 3-methyl- (CAS) $$ Prenol $$ 2-METHYL... 71 A ....... I • • । * * • * । * * 41 4.40 4.60 4.80 5.00 5000 m/z 57.00 74.92% 53 86 27 68

ol “ i “' ‘ i ■ Trp-T-rr-p-T T —m TT—wungur

A ...... • i ■ ‘ ‘ i ■ • miz—> 20 25 30 35 40 45 50 556065 70 75 80859095 Abundance #4025: 2-Penten-1-ol, (Z)- $$ cis-2-Penten-1-ol $$ cis-3-P... A T-TTTIr1—rETT1’’11113 5(7 4.40 4.60 4.80 5.00 m/z 43.10 57.01% 5000 27

miz—> 31

0 “ i"1'i1 1111 ‘ 11 20 25 30 35 —L mH 40 44

45 50 53

55 60 65 68 71 -PMPPITTTT 86 70 75 80 85 90 95 ) 0y 4.40 4.60 4.80 5.00

03517.D HP022102.M Fri Mar 15 10:09:41 2002 Page 7

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