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GCMS blank results for sample AE03508, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of a method blank for sample AE03508 to verify analytical system cleanliness.

NYC-WTC_000037635–000037654

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report v Data File : C:\MSDCHEM\l\5973N\02MAR08\03508.D Vial: 4 Acq On : 8 Mar 2002 1:07 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.611 19 21 29 rVB 41760 72967 0.47% 0.092% 2 3.927 45 49 53 rVB 21382 37878 0.24% 0.048% 3 4.243 75 77 85 rW3 30861 70114 0.45% 0.088% 4 4.638 107 112 125 rBV4 10966 53206 0.34% 0.067% 5 4.875 129 133 143 rBV3 17690 62723 0.40% 0.079% 6 5.011 143 145 153 rVB 70715 127911 0.82% 0.161% 7 5.710 203 207 213 rVB 34701 61888 0.39% 0.078% 8 5.891 219 223 243 rBV 897500 1874101 11.96% 2.353% 9 8.589 457 462 465 rBV 34718 58135 0.37% 0.073% 10 9.707 557 561' 567 rBV 4832674 9633318 61.47% 12.095% 11 9.865 573 575 579 rBV 16049 39077 0.25% 0.049% 12 9.944 579 582 591 rVB2 16491 50278 0.32% 0.063% 13 12.540 807 812 817 rVB 33686 59189 0.38% 0.074% 14 13.195 865 870 875 rBV 7073817 13944385 88.98% 17.508% 15 18.331 1319 1325 1331 rBV 7427508 14958021 95.45% 18.781% 16 22.283 1671 1675 1681 rBV 41317 84814 0.54% 0.106% 17 22.633 1701 1706 1711 rBV2 7427132 15671413 100.00% 19.677% 18 27.724 2153 2157 2161 rW 916590 1710909 10.92% 2.148% 19 30.478 2395 2401 2435 rBV 4986565 12592213 80.35% 15.810% 20 34.407 2743 2749 2785 rBV 3180400 8482083 54.12% 10.650%

Sum of corrected areas: 79644623

33508.D HP022102.M Fri Mar 15 10:08:49 2002 Page 1

NYC-WTC_000037639

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NYC-WTC_000037639Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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