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GCMS analysis results for sample AE03075, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.

NYC-WTC_000010907–000010926

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document LSC Area Percent Report v Data File : C:\MSDCHEM\l\5973N\02FEB28\02715.D Vial: 5 Acq On : 28 Feb 2002 1:50 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.622 17 22 29 rVB 35451 72280 0.51% 0.099% 2 3.927 47 49 53 rVB 20490 32989 0.23% 0.045% 3 4.096 59 64 75 rW3 7942 26016 0.18% 0.036% 4 4.254 75 78 85 rW3 27559 61880 0.44% 0.085% 5 4.378 85 89 93 rW3 8777 17059 0.12% 0.023% 6 4.638 107 112 125 rVB5 12712 41462 0.29% 0.057% 7 4.875 131 133 143 rBV3 12285 42035 0.30% 0.057% 8 5.936 225 227 247 rVB 57984 164070 1.16% 0.224% 9 9.718 557 562 567 rBV 4036683 8193845 58.00% 11.208% 10 13.195 865 870 875 rBV 6320149 12077555 85.49% 16.520% 11 13.375 883 886 895 rVB2 11352 26149 0.19% 0.036% 12 16.548 1165 1167 1171 rVB 10593 17559 0.12% 0.024% 13 18.342 1319 1326 1331 rBV 6275818 13265542 93.90% 18.145% 14 22.282 1671 1675 1681 rBV2 40517 86952 0.62% 0.119% 15 22.644 1701 1707 1711 rBV 6218262 14127828 100.00% 19.324% 16 22.768 1715 1718 1737 rVB2 79354 333997 2.36% 0.457% 17 24.856 1897 1903 1909 rBV 46058 96285 0.68% 0.132% 18 27.724 2153 2157 2163 rBV 1084679 1910999 13.53% 2.614% 19 30.489 2397- 2402 2439 rBV2 5160592 12904559 91.34% 17.651% 20 34.407 2743 2749 2787 rBV 3329594 9610007 68.02% 13.145%

Sum of corrected areas: 73109068

D2715.D HP022102.M Fri Mar 01 10:07:06 2002 Page 1

NYC-WTC_000010911

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NYC-WTC_000010911Source: NYC Law Department, mirrored locally

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