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GCMS blank results for sample AE03615, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03615 to verify analytical system cleanliness.

NYC-WTC_000037760–000037779

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03615.D Vial: 5 Acq On : 8 Mar 2002 6:52 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.498 7 11 15 rVB 50360 81604 0.51% 0.100% 2 3.622 19 22 25 rBV 37333 67198 0.42% 0.082% 3 3.769 31 35 45 rBV 10794 35032 0.22% 0.043% 4 4.243 73 77 85 rW2 32179 74201 0.47% 0.091% 5 4.638 105 112 123 rBV6 11888 52988 0.33% 0.065% 6 4.875 129 133 137 rBV2 13597 40506 0.26% 0.050% 7 5.022 143 146 151 rVB 29207 53422 0.34% 0.065% 8 5.891 219 223 231 rW 853721 1699807 10.71% 2.082% 9 6.004 231 233 247 rVB 98248 217588 1.37% 0.266% 10 8.589 459 462 469 rBV2 19654 41613 0.26% 0.051% 11 9.707 557 561 567 rBV 4791003 9498737 59.86% 11.632% 12 12.540 807 812 815 rVB 24912 46173 0.29% 0.057% 13 13.195 865 870 875 rBV 6806603 13606999 85.75% 16.663% 14 13.376 883 886 897 rVB 14025 34458 0.22% 0.042% 15 18.332 1319 1325 1331 rBV 7417948 14791911 93.22% 18.114% 16 22.283 1669 1675 1681 rVB2 41343 88634 0.56% 0.109% 17 22.633 1701 1706 1711 rBV2 7370435 15867959 100.00% 19.432% 18 27.724 2153 2157 2161 rBV 957816 1798240 11.33% 2.202% 19 30.490 2395 2402 2425 rBV 5379054 13658921 86.08% 16.727% 20 34.407 2743 2749 2793 rBV 3667301 9903324 62.41% 12.128%

Sum of corrected areas: 81659315

03515.D HP022102.M Fri Mar 15 10:09:29 2002 Page 1

NYC-WTC_000037764

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NYC-WTC_000037764Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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