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GCMS blank results for sample AE03611, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03611 to verify analytical system cleanliness.

NYC-WTC_000037700–000037719

Folder label: “GCMS X 2/19/02 A 3/8/02

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Scanned page image, NYC-WTC_000037704
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03611.D Vial: 1 Acq On : 8 Mar 2002 3 :35 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.487 7 10 15 rVB 30202 44961 0.28% 0.054% 2 3.611 19 21 25 rBV 39304 56923 0.35% 0.068% 3 4.243 75 77 85 rBV3 30347 63323 0.39% 0.076% 4 4.638 105 112 127 rBV4 12827 57915 0.36% 0.070% 5 4.875 127 133 137 rBV2 11079 41825 0.26% 0.050% 6 5.011 143 145 151 rVB 23848 45343 0.28% 0.055% 7 5.891 219 223 235 rW 787781 1831679 11.39% 2.202% 8 6.049 235 237 259 rVB 85398 273806 1.70% 0.329% 9 8.589 459 462 469 rBV 31195 71454 0.44% 0.086% 10 9.583 545 550 557 rBV4 10716 41886 0.26% 0.050%

11 9.707 557 561 573 rW 4741774 9850152 61.28% 11.842% 12 9.865 573 575 579 rW 16379 43528 0.27% 0.052% 13 9.944 579 582 593 rVB5 17276 62580 0.39% 0.075% 14 13.195 865 870 875 rBV 7078957 13938098 86.71% 16.756% 15 18.332 1319 1325 1331 rBV 7500372 14993703 93.27% 18.025% 16 22.283 1669 1675 1685 rVB 42794 89075 0.55% 0.107% 17 22.633 1701 1706 1711 rBV2 7431644 16075287 100.00% 19.325% 18 27.724 2153 2157 2161 rBV 899766 1744575 10.85% 2.097% 19 30.490 2395 2402 2447 rW 5620493 13893047 86.42% 16.702% 20 34.407 2743 2749 2783 rBV 3704835 9963241 61.98% 11.978%

Sum of corrected areas: 83182401

03511.D HP022102.M Fri Mar 15 10:09:10 2002 Page 1

NYC-WTC_000037704

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NYC-WTC_000037704Source: NYC Law Department, mirrored locally

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