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GCMS blank results for sample AE03614, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03614 to verify analytical system cleanliness.

NYC-WTC_000037740–000037759

Folder label: “GCMS X 2/19/02 A 3/8/02

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Scanned page image, NYC-WTC_000037744
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NYC 9/11 Public Portal Document LSC Area Percent Report . Data File : C:\MSDCHEM\1\5973N\02MAR08\03614.D Vial: 4 Acq On : 8 Mar 2002 6:03 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.487 5 10 15 rVB 33743 57534 0.36% 0.070% 2 3.611 17 21 29 rVB 38379 67983 0.43% 0.083% 3 3.916 45 48 53 rVB 17849 34407 0.22% 0.042% 4 4.243 75 77 85 rVB2 30327 60771 0.38% 0.074% 5 4.638 107 112 125 rVB7 10737 51119 0.32% 0.062% 6 4.875 125 133 137 rBV4 15870 45050 0.28% 0.055% 7 5.022 143 146 151 rVB 26429 51413 0.32% 0.063% 8 5.891 219 223 231 rBV 814570 1670602 10.45% 2.035% 9 6.004 231 233 251 rW 69216 181201 1.13% 0.221% 10 8.589 457 462 465 rW 33833 57525 0.36% 0.070% 11 9.707 557 561 567 rBV 4801727 9576904 59.88% 11.668% 12 9.955 579 583 591 rVB3 14628 41407 0.26% 0.050% 13 13.195 865 870 875 rBV 6953653 13792454 86.24% 16.804% 14 13.376 883 886 891 rVB2 15242 31412 0.20% 0.038% 15 18.332 1319 1325 1331 rBV 7628755 14897780 93.15% 18.151% 16 22.283 1669 1675 1683 rVB 43825 88325 0.55% 0.108% 17 22.633 1701 1706 1711 rBV2 7445157 15993510 100.00% 19.486% 18 27.724 2151 2157 2161 rBV 935874 1751469 10.95% 2.134% 19 30.490 2395 2402 2453 rW 5446998 13813849 86.37% 16.830% 20 34.407 2743 2749 2783 rBV 3727137 9813187 61.36% 11.956%

Sum of corrected areas: 82077902

03514.D HP022102.M Fri Mar 15 10:09:22 2002 Page 1

NYC-WTC_000037744

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NYC-WTC_000037744Source: NYC Law Department, mirrored locally

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