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GCMS blank results for sample AE03509, March 28, 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of a method blank for sample AE03509 to verify analytical system cleanliness.

NYC-WTC_000037660–000037679

Folder label: “GCMS X 2/19/02 A 3/8/02

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Scanned page image, NYC-WTC_000037664
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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03509.D Vial: 5 Acq On : 8 Mar 2002 1:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.622 19 22 29 rBV 39980 73293 0.44% 0.083% 2 3.927 47 49 53 rVB 23309 37685 0.23% 0.043% 3 4.243 75 77 85 rVB2 56861 116720 0.70% 0.133% 4 4.638 105 112 125 rBV3 14315 56717 0.34% 0.065% 5 4.875 129 133 143 rBV5 14771 61799 0.37% 0.070% 6 5.011 143 145 153 rVB 57771 111098 0.67% 0.126% 7 5.711 203 207 213 rVB 28205 55983 0.34% 0.064% 8 5.891 219 223 239 rBV 895807 1891240 11.35% 2.152% 9 6.083 239 240 249 rVB2 19639 54675 0.33% 0.062% 10 8.589 457 462 465 rBV 33715 62543 0.38% 0.071% 11 9.707 557 561 567 rBV 5270690 10207284 61.26% 11.616% 12 9.944 573 582 593 rVB3 14907 62668 0.38% 0.071% 13 13.195 865 870 875 rBV 7524630 14848820 89.12% 16.898% 14 18.332 1319 1325 1331 rBV 7917525 15777675 94.70% 17.955% 15 22.283 1671 1675 1681 rW 52819 103300 0.62% 0.118% 16 22.633 1701 1706 1711 rBV2 7670639 16661411 100.00% 18.960% 17 22.768 1715 1718 1729 rVB 75277 239727 1.44% 0.273% 18 27.724 2151 2157 2161 rBV 988619 1875828 11.26% 2.135% 19 30.490 2395 2402 2433 rBV 5954099 14515950 87.12% 16.519% 20 34.407 2743 2749 2777 rBV 4313952 11060485 66.38% 12.587%

Sum of corrected areas: 87874901

03509.D HP022102.M Fri Mar 15 10:08:56 2002 Page 1

NYC-WTC_000037664

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NYC-WTC_000037664Source: NYC Law Department, mirrored locally

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