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GCMS analysis results for sample AE03617, March 28, 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AE03617 conducted on March 28, 2002.

NYC-WTC_000037800–000037818

Folder label: “GCMS X 2/19/02 A 3/8/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02MAR08\03517.D Vial: 7 Acq On : 8 Mar 2002 8:31 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % Of # min scan scan scan TY height area % max. total 1 3.498 9 11 15 rVB 68593 96835 0.52% 0.098% 2 3.622 19 22 25 rBV 44096 79543 0.43% 0.081% 3 3.927 47 49 53 rBV 29688 44222 0.24% 0.045% 4 4.254 75 78 85 rW4 36705 86192 0.47% 0.088% 5 4.649 103 113 121 rBV5 18125 72981 0.40% 0.074%

6 4.864 127 132 137 rBV2 24936 70434 0.38% 0.072% 7 5.022 143 146 151 rW 41671 74638 0.40% 0.076% 8 5.891 219 223 231 rBV 1126737 2241864 12.15% 2.278% 9 6.004 231 233 239 rVB 102311 197028 1.07% 0.200% 10 8.589 459 462 469 rW2 22157 50378 0.27% 0.051% 11 9.707 557 561 567 rBV 5819967 11580178 62.73% 11.768% 12 13.195 865 870 875 rBV 8420770 16749380 90.74% 17.021% 13 18.332 1319 1325 1331 rBV 8619603 17763404 96.23% 18.052% 14 22.283 1671 1675 1681 rBV 55016 116175 0.63% 0.118% 15 22.633 1701 1706 1711 TBV2 8198303 18458958 100.00% 18.759% 16 22.768 1715 1718 1739 rVB2 88670 357488 1.94% 0.363% 17 27.724 2151 2157 2161 rBV 1174105 2289859 12.41% 2.327% 18 30.490 2395 2402 2407 rBV 6526152 15243289 82.58% 15.491% 19 31.088 2451 2455 2479 rVB 54419 230834 1.25% 0.235% 20 34.407 2743 2749 2791 rW 4801484 12599305 68.26% 12.804%

Sum of corrected areas: 98402985

03517.D HP022102.M Fri Mar 15 10:09:40 2002 Page 1

NYC-WTC_000037804

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NYC-WTC_000037804Source: NYC Law Department, mirrored locally

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