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GCMS analysis results for sample AE02713, March 5 2002

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Laboratory report documenting gas chromatography-mass spectrometry results for sample AE02713 including surrogate recovery.

NYC-WTC_000010867–000010886

Folder label: “GCMS X 2/5/02 A 2/28/02

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NYC 9/11 Public Portal Document LSC Area Percent Report Data File : C:\MSDCHEM\1\5973N\02FEB28\02713.D Vial: 3 Acq On : 28 Feb 2002 12:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.611// 19 21 29 rBV 34102 58932 0.49% 0.094% 2 3.916 45 48 53 rVB 15104 26319 0.22% 0.042% 3 4.006 53 56 67 rVB2 5200 18448 0.15% 0.029% 4 4.254/ 73 78 85 rVB6 5168 23619 0.20% 0.038% 5 4.638/ 107 112 119 rVB3 7574 18997 0.16% 0.030% 6 5.5074 185 189 199 rVB3 3307 11950 0.10% 0.019% 7 5.936/ 225 227 237 rBV 48659 130387 1.08% 0.208% 8 9.707 557 561 575 rW 3537868 7416377 61.55% 11.858% 9 13.195 / 865 870 875 rBV 5478156 10627684 88.20% 16.993% 10 13.376/ 883 886 901 rVB3 10815 33222 0.28% 0.053% 11 16.548 1163 1167 1175 rBV2 6536 15158 0.13% 0.024% 12 18.332 1319 1325 1331 rBV 5580907 11530866 95.69% 18.437% 13 22.283 1671 1675 1681 rBV 30662 59076 0.49% 0.094% 14 22.633 1701 1706 1711 rBV2 5506347 12050116 100.00% 19.267% 15 24.857 1897 1903 1909 rBV 13592 33312 0.28% 0.053% 16 26.177 2017 2020 2027 rBV2 22454 44003 0.37% 0.070% 17 27.724 2153 2157 2163 rW 744460 1263874 10.49% 2.021% 18 30.490 2397 2402 2423 rBV 4582027 10911516 90.55% 17.447% 19 34.407 2743 2749 2787 rBV 2951046 8248864 68.45% 13.189% 20 35.378/2831 2835 2841 rBV4 5514 19382 0.16% 0.031%

Sum of corrected areas: 62542102

02713.D HP022102.M Fri Mar 01 10:06:52 2002 Page 1

NYC-WTC_000010872

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NYC-WTC_000010872Source: NYC Law Department, mirrored locally

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