GCMS analysis results, Feb 27 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C : \MSDCHEM\1\5973N\02FEB25\ 01136 .D Vial: 3 Acq On : 25 Feb 2002 12:53 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 20 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.509 9 12 17 rBV 36204 62165 0.47% 0.088% 2 3.634 21 23 29 rBV 34515 66477 0.50% 0.094% 3 3.938 47 50 55 rVB 19218 29247 0.22% 0.041% 4 4.390 87 90 93 rBV 18631 33763 0.25% 0.048% 5 5.135 151 156 165 rBV5 6027 21609 0.16% 0.031%

6 5.948 225 228 239 rBV2 51220 206580 1.55% 0.292% 7 9.707 557 561 567 rBV 4085522 8214500 61.50% 11.612% 8 12.540 807 812 817 rVB 59415 104521 0.78% 0.148% 9 13.195 865 870 875 rBV 6015800 11907842 89.15% 16.832% 10 13.376 883 886 901 rVB2 21211 55873 0.42% 0.079%

11 16.548 1161 1167 1173 rBV2 9579 23269 0.17% 0.033% 12 18.332 1319 1325 1331 rBV 6264551 12743640 95.41% 18.014% 13 18.738 1355 1361 1369 rVB4 5581 22782 0.17% 0.032% 14 22.283 1669 1675 1679 rBV2 38355 76734 0.57% 0.108% 15 22.633 1701 1706 1711 rBV2 6139577 13357119 100.00% 18.881%

16 24.857 1899 1903 1911 rBV 20664 50916 0.38% 0.072% 17 27.724 2151 2157 2163 rBV 863660 1552898 11.63% 2.195% 18 30.490 2397 2402 2437 rBV2 5007760 12254951 91.75% 17.323% 19 31.099 2451 2456 2467 rBV 68539 197608 1.48% 0.279% 20 34.407 2743 2749 2781 rBV 3529941 9761813 73.08% 13.799%

Sum of corrected areas: 70744307

01136 .D HP022102 .M Tue Feb 26 08:29:55 2002 Page 1

NYC-WTC_000003448