GCMS analysis results for sample AE03075, March 5 2002

NYC 9/11 Public Portal Document LSC Area Percent Report

v Data File : C:\MSDCHEM\l\5973N\02FEB28\02716 .D Vial: 1 Acq On : 28 Feb 2002 2:40 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 28, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\MSDCHEM\1\METHODS\METHODS\HP022102.M (RTE Integrator) Title : 508 scan method Smoothing : OFF Filtering: 5 Sampling : 2 Min Area: 100 Area counts Start Thrs: 0.2 Max Peaks: 2 0 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total 1 3.611 19 21 31 rVB 26626 50459 0.40% 0.077% 2 3.927 45 49 53 rBV 17004 28562 0.23% 0.044% 3 4.243 73 77 85 rW3 69596 128314 1.01% 0.197% 4 5.022 143 146 151 rBV3 13502 29102 0.23% 0.045% 5 5.722 205 208 213 rVB4 7244 13724 0.11% 0.021%

6 5.948 223 228 249 rVB 32715 107145 0.84% 0.164% 7 9.718 557 562 567 rBV 3612595 7355022 57.94% 11.279% 8 13.195 865 870 875 rBV 5577545 10780971 84.93% 16.533% 9 13.376 883 886 891 rVB2 10002 25450 0.20% 0.039% 10 16.548 1163 1167 1173 rBV3 9604 21076 0.17% 0.032% 11 18.332 1319 1325 1331 rBV 5672087 11831537 93.20% 18.144% 12 18.727 1357 1360 1367 rVB4 4414 15611 0.12% 0.024% 13 22.283 1669 1675 1679 rBV 37706 75603 0.60% 0.116% 14 22.633 1701 1706 1711 rBV2 5784305 12694180 100.00% 19.467% 15 22.768 1715 1718 1751 rVB 74486 396144 3.12% 0.607% 16 24.857 1899 1903 1907 rBV 22991 47657 0.38% 0.073% 17 27.724 2153 2157 2163 rBV 911885 1601364 12.61% 2.456% 18 30.490 2397 2402 2441 rBV 4794175 11517042 90.73% 17.661% 19 33.639 2671 2681 2683 rBV4 3155 17248 0.14% 0.026% 20 34.407 2743 2749 2783 rBV 2975757 8473812 66.75% 12.995%

Sum of corrected areas: 65210023

02716.D HP022102.M Fri Mar 01 10:07:13 2002 Page 1

NYC-WTC_000010931