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GCMS analysis results for sample AD29564, Jan 2002

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GCMS analysis report for sample AD29564 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036915–000036926

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\DEC3101\29564.D Vial: 62 Operator: 209 GALOS Acq On Sample 3 Jan 2002 gems scan 12/7 2:02 am C Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 3 2:51 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 1421036 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 5494218 20.00 ug/1 -0.02 17) Acenaphthene-dlO 20.56 164 2754608 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 3948719 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 2600890 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 1539189 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 150167 3 .4 g/mL 0.00 Spiked Amount 5.000 Recovery 69.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.29 74 812 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 11.13 146 568 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.39 77 208 N.D. 12) Isophorone 14.31 82 1760 N.D. 13) bis(2-Chloroethoxy)methane 14.33 93 690 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 2096 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.47 162 458 N.D. 20) Dimethylphthalate 20.28 163 7381 N.D. 21) 2,6-Dinitrotoluene 20.28 165 3872 N.D. 2 2) Acenaphthylene 20.28 152 1058 N.D. 23) Acenaphthene 20.29 153 232 N.D. 24) 2,4-Dinitrotoluene 21.35 165 •592 N.D. 25) Diethylphthalate 22.11 149 1803 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29564 .D GCMS1126 .M Tue Jan 15 16:07:51 2002 Page 1

NYC-WTC_000036917

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NYC-WTC_000036917Source: NYC Law Department, mirrored locally

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