NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\JAN0302\29670.D Vial: 15
Acq On 4 Jan 2002 12:13 am Operator: 209 GALOS
Sample gems scan 12/7 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 4 1:02 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Fri Dec 28 15:11:00 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.53 152 1456044 20.00 ug/1 -0.17
10) Naphthalene-d8 15.13 136 5560634 20.00 ug/1 -0.18
17) Acenaphthene-diO 20.40 164 2675296 20.00 ug/1 -0.18
29) Phenanthrene-diO 24.81 188 3953832 20.00 ug/1 -0.18
38) Chrysene-dl2 32.85 240 2292948 20.00 ug/1 -0.19
44) Perylene-dl2 36.91 264 1342805 20.00 ug/1 -0.21
System Monitoring Compounds
37) 2,4-DDD 29.88 235 161920 3.72 ug/mL -0.19
Spiked Amount 5.000 Recovery = 74.40%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 0.00 74 ■ 0 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,21 -oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 12.93 77 421 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.17 128 344 0 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.05 165 493 N.D.
25) Diethylphthalate 21.91 149 1026 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
29670.D GCMS1126.M Tue Jan 15 15:58:01 2002 Page 1
NYC-WTC_000036844
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