NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\DEC3101\30694.D Vial: 31
Acq On 1 Jan 2002 6:01 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 18 11:04 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title •: 209 625/TCLP calibration table
Last Update : Fri Dec 28 15:11:00 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 779603 20.00 ug/1 -0.03
10) Naphthalene-d8 15.28 136 2973327 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.56 164 1499835 20.00 ug/1 -0.02
29) Phenanthrene-diO 24.98 188 2153370m 20.00 ug/1 0.00
38) Chrysene-dl2 33.02 240 1286733 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 700659 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.07 235 115371 4.87 ug/mL 0.00
Spiked Amount 5.000 Recovery = 97.40%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.25 74 189 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.34 128 459 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 0.00 163 0 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.24 165 272 N.D.
25) Diethylphthalate 22.16 149 1621 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
2 7) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30694.D GCMS1126.M Fri Jan 18 11:05:14 2002 Page 1
NYC-WTC_000018095
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