NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\DEC3101\30605.D Vial: 30
Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 18 11:31 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update • : Fri Dec 28 15:11:00 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 815257 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 3167895 20.00 ug/1 -0.02
17) Acenaphthene-dl0 20.56 164 1618752 20.00 ug/1 -0.01
29) Phenanthrene-diO 24.99 188 2339060m 20.00 ug/1 0.00
38) Chrysene-dl2 33.03 240 1411367 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 780271 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.06 235 142749 5.55 ug/mL 0.00
Spiked Amount 5.000 Recovery = 111.00%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.23 74 468 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichiorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D. »
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.33 128 576 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 20.28 163 299 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
2 3) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.42 165 171 N.D.
25) Diethylphthalate 22.14 149 2705 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
2 7) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30605.D GCMS1126.M Fri Jan 18 11:32:11 2002 Page 1
NYC-WTC_000018196
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