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GCMS analysis log for sample AD30605, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.

NYC-WTC_000018194–000018213

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\DEC3101\30605.D Vial: 30 Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 18 11:31 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update • : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.06 178 209 N.D. 34) Anthracene 25.06 178 209 N.D. 35) Di-n-butylphthalate 27.05 149 7408 N.D. 3 6) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.54 149 424 N.D. 41) Benzo(a)anthracene 33.02 228 4413 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 10518 N.D. 43) Chrysene 33.02 228 4413 N.D. 45) Di-n-Octylphthalate 35.05 149 314 N.D. 46) Benzo(b)fluoranthene 36.12 252 171 N.D. 47) Benzo(k)fluoranthene 36.12 252 171 N.D. 4 8) Benzo(a)pyrene 37.13 252 3489 N.D. ' 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30605.D GCMS1126.M Fri Jan 18 11:32:15 2002 Page 2

NYC-WTC_00001 8197

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NYC-WTC_000018197Source: NYC Law Department, mirrored locally

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