GCMS analysis log for sample AD30712, Jan 2002

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Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.

NYC-WTC_000018214–000018237

Folder label: “GCMS X 12/27/01 A 1/16/02”

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\30712.D Vial: 35 Acq On 1 Jan 2002 9:53 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 1 22:42 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update • : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 660688 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 2526347 20.00 ug/1 -0.02 17) Acenaphthene-diO 20.56 164 1279116 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 1862745 20.00 ug/1 0.00 38) Chrysene-dl2 33.03 240 1117703 20.00 ug/1 0.00 44) Perylene-dl2 37.12 264 619406 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.06 235 104491 5.10 ug/mL 0.00 Spiked Amount 5.000 Recovery = 102.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-ChloroprOpan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 570 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.28 163 794 N.D. 21) 2,6-Dinitrotoluene 20.28 165 295 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.17 165 365 N.D. 25) Diethylphthalate 22.14 149 2512 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 30712.D GCMS1126.M Wed Jan 23 11:33:29 2002 Page 1

NYC-WTC_000018216

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