NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C: \HPCHEM\ 1 \DATA\DEC3101\30714.D Vial: 29
Acq On 1 Jan 2002 4:05 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Jan 18 11:30 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title • : 209 625/TCLP calibration table
Last Update : Fri Dec 28 15:11:00 2001
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 879771 20.00 ug/1 -0.03
10) Naphthalene-d8 15.28 136 3367875 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.56 164 1715837 20.00 ug/1 -0.02
29) Phenanthrene-diO 24.98 188 2491021m 20.00 ug/1 0.00
38) Chrysene-dl2 33.02 240 1432985 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 800051 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.07 235 127055 4.64 ug/mL 0.00
Spiked Amount 5.000 Recovery = 92.80%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.29 74 199 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybi s(1-Chioropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachioroethane 0.00 117 0 N.D.
11) Nitrobenzene 13.78 77 107 N.D.
12) 1sophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.33 128 253 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachiorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 20.27 163 484 N.D.
21) 2,6-Dinitrotoluene 20.27 165 214 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.26 165 289 N.D.
25) Diethylphthalate 22.14 149 1749 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30714.D GCMS1126.M Fri Jan 18 11:30:52 2002 Page 1
NYC-WTC_000018176
OCR can misread numbers and units. Confirm readings against the page image before using them.