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GCMS analysis results for sample AD29564, Jan 2002

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GCMS analysis report for sample AD29564 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036915–000036926

Folder label: “GCMS X 12/7/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\DEC3101\29564.D Vial: 62 Acq On 3 Jan 2002 2:02 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 3 2:51 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.95 178 3263 N.D. 34) Anthracene 24.95 178 3263 N.D. 35) Di-n-butylphthalate 27.02 149 36458 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.50 149 1502 N.D. 41) Benzo(a)anthracene 33.02 228 7208 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 16198 N.D. 43) Chrysene 33.02 228 7208 N.D. 45) Di-n-Octylphthalate 35.05 149 1645 N.D. 46) Benzo(b)fluoranthene 36.09 252 305 N.D. 47) Benzo(k)fluoranthene 36.20 252 894 N.D. 48) Benzo(a)pyrene 36.97 252 289 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29564.D GCMS1126.M Tue Jan 15 16:07:55 2002. Page 2

NYC-WTC_000036918

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NYC-WTC_000036918Source: NYC Law Department, mirrored locally

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